C₁₅H₇⁽²⁾H₅Cl₂

Base Information

Chemical Name:C₁₅H₇⁽²⁾H₅Cl₂
CAS No.:1416227-53-6
Molecular Formula:C₁₅H₁₂Cl₂
Molecular Weight:268.127
Hs Code.:

C<sub>15</sub>H<sub>7</sub><sup>(2)</sup>H<sub>5</sub>Cl<sub>2</sub>

Synonyms:C₁₅H₇⁽²⁾H₅Cl₂

Suppliers and Price of C₁₅H₇⁽²⁾H₅Cl₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₅H₇⁽²⁾H₅Cl₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₅H₇⁽²⁾H₅Cl₂

There total 16 articles about C₁₅H₇⁽²⁾H₅Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1416227-31-0
(1S,3S)-6-chloro-3-(phenyl-d₅)-indan-1-ol

: 1416227-53-6
C₁₅H₇⁽²⁾H₅Cl₂

Guidance literature:: With thionyl chloride; In tetrahydrofuran; at 20 ℃; Product distribution / selectivity;

Reference yield:

: 4165-57-5
bromobenzene-d5

: 1416227-53-6
C₁₅H₇⁽²⁾H₅Cl₂

Guidance literature:: Multi-step reaction with 5 steps

1: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / dichloromethane; ISOPROPYLAMIDE; 2-methyltetrahydrofuran / 3 h / 80 - 85 °C / Industry scale

2: triethylamine; cyclo-octa-1,5-diene / bis(norbornadiene)rhodium(l)tetrafluoroborate / 1,4-dioxane / 5 h / 48 - 53 °C / Industry scale

3: sodium tetrahydroborate / tetrahydrofuran / 5 h / -35 - 20 °C / Industry scale

4: vinyl n-butyrate; Novozym-435 / di-isopropyl ether

5: thionyl chloride / tetrahydrofuran / 20 °C

With sodium tetrahydroborate; thionyl chloride; vinyl n-butyrate; Novozym-435; potassium acetate; triethylamine; cyclo-octa-1,5-diene; bis(norbornadiene)rhodium(l)tetrafluoroborate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; 2-methyltetrahydrofuran; 1,4-dioxane; dichloromethane; di-isopropyl ether; ISOPROPYLAMIDE;

Reference yield:

: 80272-44-2
3-bromo-6-chloro-1-indanone

: 1416227-53-6
C₁₅H₇⁽²⁾H₅Cl₂

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / tetrahydrofuran / 8 h / 0 - 5 °C / Industry scale

2: triethylamine; cyclo-octa-1,5-diene / bis(norbornadiene)rhodium(l)tetrafluoroborate / 1,4-dioxane / 5 h / 48 - 53 °C / Industry scale

3: sodium tetrahydroborate / tetrahydrofuran / 5 h / -35 - 20 °C / Industry scale

4: vinyl n-butyrate; Novozym-435 / di-isopropyl ether

5: thionyl chloride / tetrahydrofuran / 20 °C

With sodium tetrahydroborate; thionyl chloride; vinyl n-butyrate; Novozym-435; triethylamine; cyclo-octa-1,5-diene; bis(norbornadiene)rhodium(l)tetrafluoroborate; In tetrahydrofuran; 1,4-dioxane; di-isopropyl ether;