4'-methoxyphenyl (R,R)-3-[N-phenyl-N-(α-methylbenzyl)amino]-5-methylhexanoate

Base Information

Chemical Name:4'-methoxyphenyl (R,R)-3-[N-phenyl-N-(α-methylbenzyl)amino]-5-methylhexanoate
CAS No.:1296207-63-0
Molecular Formula:C₂₈H₃₃NO₃
Molecular Weight:431.575
Hs Code.:

Synonyms:4'-methoxyphenyl (R,R)-3-[N-phenyl-N-(α-methylbenzyl)amino]-5-methylhexanoate

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Chemical Property of 4'-methoxyphenyl (R,R)-3-[N-phenyl-N-(α-methylbenzyl)amino]-5-methylhexanoate

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Technology Process of 4'-methoxyphenyl (R,R)-3-[N-phenyl-N-(α-methylbenzyl)amino]-5-methylhexanoate

There total 4 articles about 4'-methoxyphenyl (R,R)-3-[N-phenyl-N-(α-methylbenzyl)amino]-5-methylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1296207-53-8
4''-methoxyphenyl (E)-5-methylhex-2-enoate

: 779-54-4,21232-36-0,21232-37-1,23652-68-8
(R)-phenyl-(1-phenylethyl)amine

: 1296207-63-0
4'-methoxyphenyl (R,R)-3-[N-phenyl-N-(α-methylbenzyl)amino]-5-methylhexanoate

Guidance literature:: (R)-phenyl-(1-phenylethyl)amine; With n-butyllithium; In tetrahydrofuran; hexanes; at -78 ℃; Inert atmosphere;

4''-methoxyphenyl (E)-5-methylhex-2-enoate; In tetrahydrofuran; hexanes; at -78 ℃; for 2h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol200625h

Reference yield:

: 3886-69-9
(R)-1-phenyl-ethyl-amine

: 1296207-63-0
4'-methoxyphenyl (R,R)-3-[N-phenyl-N-(α-methylbenzyl)amino]-5-methylhexanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: cesium fluoride / acetonitrile / 16 h / 60 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexanes / -78 °C / Inert atmosphere

2.2: 2 h / -78 °C / Inert atmosphere

With n-butyllithium; cesium fluoride; In tetrahydrofuran; hexanes; acetonitrile;
DOI:10.1021/ol200625h

Reference yield:

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 1296207-63-0
4'-methoxyphenyl (R,R)-3-[N-phenyl-N-(α-methylbenzyl)amino]-5-methylhexanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: cesium fluoride / acetonitrile / 16 h / 60 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexanes / -78 °C / Inert atmosphere

2.2: 2 h / -78 °C / Inert atmosphere

With n-butyllithium; cesium fluoride; In tetrahydrofuran; hexanes; acetonitrile;
DOI:10.1021/ol200625h