1-[(6-triethoxysilyl-3-oxahexyl)]-4-(methyldiphenylphosphine-borane)-1H-1,2,3-triazole

Base Information

Chemical Name:1-[(6-triethoxysilyl-3-oxahexyl)]-4-(methyldiphenylphosphine-borane)-1H-1,2,3-triazole
CAS No.:1537217-85-8
Molecular Formula:C₂₆H₄₁BN₃O₄PSi
Molecular Weight:529.5
Hs Code.:

Synonyms:1-[(6-triethoxysilyl-3-oxahexyl)]-4-(methyldiphenylphosphine-borane)-1H-1,2,3-triazole

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Chemical Property of 1-[(6-triethoxysilyl-3-oxahexyl)]-4-(methyldiphenylphosphine-borane)-1H-1,2,3-triazole

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Technology Process of 1-[(6-triethoxysilyl-3-oxahexyl)]-4-(methyldiphenylphosphine-borane)-1H-1,2,3-triazole

There total 4 articles about 1-[(6-triethoxysilyl-3-oxahexyl)]-4-(methyldiphenylphosphine-borane)-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 906543-22-4
propargyl(diphenyl)phosphine borane complex

: 1110650-81-1
1-triethoxysilyl-4-oxa-6-azidohexane

: 1537217-85-8
1-[(6-triethoxysilyl-3-oxahexyl)]-4-(methyldiphenylphosphine-borane)-1H-1,2,3-triazole

Guidance literature:: With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1080/00397911.2013.822514

Reference yield:

: 50563-72-9
2-(allyloxy)ethyl 4-methylbenzenesulfonate

: 1537217-85-8
1-[(6-triethoxysilyl-3-oxahexyl)]-4-(methyldiphenylphosphine-borane)-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 3 steps

1: Karstedt’s catalyst / tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene / 2 h / 20 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 12 h / 60 °C / Inert atmosphere

3: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

With copper(l) iodide; sodium azide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; N,N-dimethyl-formamide;
DOI:10.1080/00397911.2013.822514

Reference yield:

: 163655-63-8
C₁₈H₃₂O₇SSi

: 1537217-85-8
1-[(6-triethoxysilyl-3-oxahexyl)]-4-(methyldiphenylphosphine-borane)-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 12 h / 60 °C / Inert atmosphere

2: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

With copper(l) iodide; sodium azide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1080/00397911.2013.822514