methyl 4-(3-(N,N-diethylsulfamoyl)benzamido)-[1,1'-biphenyl]-3-carboxylate

Base Information

Chemical Name:methyl 4-(3-(N,N-diethylsulfamoyl)benzamido)-[1,1'-biphenyl]-3-carboxylate
CAS No.:1448009-54-8
Molecular Formula:C₂₅H₂₆N₂O₅S
Molecular Weight:466.558
Hs Code.:

Synonyms:methyl 4-(3-(N,N-diethylsulfamoyl)benzamido)-[1,1'-biphenyl]-3-carboxylate

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Chemical Property of methyl 4-(3-(N,N-diethylsulfamoyl)benzamido)-[1,1'-biphenyl]-3-carboxylate

Chemical Property:

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Technology Process of methyl 4-(3-(N,N-diethylsulfamoyl)benzamido)-[1,1'-biphenyl]-3-carboxylate

There total 3 articles about methyl 4-(3-(N,N-diethylsulfamoyl)benzamido)-[1,1'-biphenyl]-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 3-(N,N-diethylsulfamoyl)benzoyl chloride

: 243989-52-8
4-amino-biphenyl-3-carboxylic acid methyl ester

: 1448009-54-8
methyl 4-(3-(N,N-diethylsulfamoyl)benzamido)-[1,1'-biphenyl]-3-carboxylate

Guidance literature:: With pyridine;
DOI:10.1021/jm4006302

Reference yield:

: 1576-46-1
<(Diethylamino)sulfonyl>benzoic Acid

: 1448009-54-8
methyl 4-(3-(N,N-diethylsulfamoyl)benzamido)-[1,1'-biphenyl]-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 20 °C

2: pyridine

With pyridine; thionyl chloride; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/jm4006302

Reference yield:

: 4025-64-3
3-Carboxybenzenesulfonyl chloride

: 1448009-54-8
methyl 4-(3-(N,N-diethylsulfamoyl)benzamido)-[1,1'-biphenyl]-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 0 - 20 °C

2: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 20 °C

3: pyridine

With pyridine; thionyl chloride; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/jm4006302