2-[(1Z)-3-hydroxy-1-propenyl]phenylisothiocyanate

Base Information

Chemical Name:2-[(1Z)-3-hydroxy-1-propenyl]phenylisothiocyanate
CAS No.:224315-42-8
Molecular Formula:C₁₀H₉NOS
Molecular Weight:191.254
Hs Code.:

Synonyms:2-[(1Z)-3-hydroxy-1-propenyl]phenylisothiocyanate

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Chemical Property of 2-[(1Z)-3-hydroxy-1-propenyl]phenylisothiocyanate

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Technology Process of 2-[(1Z)-3-hydroxy-1-propenyl]phenylisothiocyanate

There total 5 articles about 2-[(1Z)-3-hydroxy-1-propenyl]phenylisothiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 91-22-5
quinoline

: 463-71-8
thiophosgene

: 224315-42-8
2-[(1Z)-3-hydroxy-1-propenyl]phenylisothiocyanate

Guidance literature:: quinoline; thiophosgene; With sodium carbonate; In tetrahydrofuran; water; at -10 ℃; for 0.333333h;

With sodium tetrahydroborate; In tetrahydrofuran; water;
DOI:10.1021/ja046407b

Reference yield: 11.36%

: 19908-02-2
3-Isothiocyanato-cis-zimtaldehyd

: 224315-42-8
2-[(1Z)-3-hydroxy-1-propenyl]phenylisothiocyanate

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; at -15 ℃;
DOI:10.1021/ol990749i

Reference yield:

: 615-43-0
2-iodophenylamine

: 224315-42-8
2-[(1Z)-3-hydroxy-1-propenyl]phenylisothiocyanate

Guidance literature:: Multi-step reaction with 3 steps

1: PdCl₂(PPh₃)2, CuI, Et₂NH

2: Zn, Br(CH₂)2Br / ethanol

3: CaCO₃

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; ethylene dibromide; diethylamine; calcium carbonate; zinc; In ethanol;
DOI:10.1021/ja983681v