C₃₆H₃₅N₅O₉

Base Information

Chemical Name:C₃₆H₃₅N₅O₉
CAS No.:1255142-85-8
Molecular Formula:C₃₆H₃₅N₅O₉
Molecular Weight:681.702
Hs Code.:

C<sub>36</sub>H<sub>35</sub>N<sub>5</sub>O<sub>9</sub>

Synonyms:C₃₆H₃₅N₅O₉

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Chemical Property of C₃₆H₃₅N₅O₉

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Technology Process of C₃₆H₃₅N₅O₉

There total 3 articles about C₃₆H₃₅N₅O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1255142-97-2
C₃₈H₃₉N₅O₉

: 1255142-85-8
C₃₆H₃₅N₅O₉

Guidance literature:: C₃₈H₃₉N₅O₉; With potassium hydroxide; In 1,4-dioxane; methanol; for 15h;

With hydrogenchloride; acetic acid; In water;
DOI:10.1002/anie.201002907

Reference yield:

: 1255142-89-2
2-bromo-6-(N-(tert-butoxycarbonyl)methyl-N-methylamino)naphthalene

: 1255142-85-8
C₃₆H₃₅N₅O₉

Guidance literature:: Multi-step reaction with 4 steps

1.1: triphenylphosphine; caesium carbonate / palladium diacetate; copper(l) iodide / N,N-dimethyl-formamide / 12 h / 140 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 24 h / Inert atmosphere

3.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 1 h

3.2: 12 h / Inert atmosphere

4.1: potassium hydroxide; methanol / 1,4-dioxane / 15 h

With methanol; benzotriazol-1-ol; caesium carbonate; dicyclohexyl-carbodiimide; triphenylphosphine; trifluoroacetic acid; potassium hydroxide; copper(l) iodide; palladium diacetate; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 305835-80-7
6-(methylamino)-2-bromonaphthalene

: 1255142-85-8
C₃₆H₃₅N₅O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetonitrile / 12 h / Proton sponge; Inert atmosphere

2.1: triphenylphosphine; caesium carbonate / palladium diacetate; copper(l) iodide / N,N-dimethyl-formamide / 12 h / 140 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 24 h / Inert atmosphere

4.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 1 h

4.2: 12 h / Inert atmosphere

5.1: potassium hydroxide; methanol / 1,4-dioxane / 15 h

With methanol; benzotriazol-1-ol; caesium carbonate; dicyclohexyl-carbodiimide; triphenylphosphine; trifluoroacetic acid; potassium hydroxide; copper(l) iodide; palladium diacetate; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; acetonitrile;