ethyl 3-(1,3-dimethyl-2,4-dioxo-5-phenyl-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)-4-hydroxybenzoate

Base Information

Chemical Name:ethyl 3-(1,3-dimethyl-2,4-dioxo-5-phenyl-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)-4-hydroxybenzoate
CAS No.:1314872-90-6
Molecular Formula:C₂₃H₂₁N₃O₅
Molecular Weight:419.437
Hs Code.:

Synonyms:ethyl 3-(1,3-dimethyl-2,4-dioxo-5-phenyl-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)-4-hydroxybenzoate

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Chemical Property of ethyl 3-(1,3-dimethyl-2,4-dioxo-5-phenyl-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)-4-hydroxybenzoate

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Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of ethyl 3-(1,3-dimethyl-2,4-dioxo-5-phenyl-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)-4-hydroxybenzoate

There total 2 articles about ethyl 3-(1,3-dimethyl-2,4-dioxo-5-phenyl-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)-4-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 626-48-2
6-Methyluracil

: 1314872-90-6
ethyl 3-(1,3-dimethyl-2,4-dioxo-5-phenyl-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)-4-hydroxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / water / 72 h / 25 °C

2: zinc(II) chloride / chlorobenzene / 3 h / Reflux

3: water; bromine / tetrachloromethane; dichloromethane / 0.17 h / 50 °C

4: ethanol / 2 h / Reflux

With water; bromine; sodium hydroxide; zinc(II) chloride; In tetrachloromethane; ethanol; dichloromethane; water; chlorobenzene; 2: Friedel Crafts acylation;
DOI:10.1021/jm200505e

Reference yield:

: 13509-52-9
1,3,6-trimethyluracil

: 1314872-90-6
ethyl 3-(1,3-dimethyl-2,4-dioxo-5-phenyl-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)-4-hydroxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: zinc(II) chloride / chlorobenzene / 3 h / Reflux

2: water; bromine / tetrachloromethane; dichloromethane / 0.17 h / 50 °C

3: ethanol / 2 h / Reflux

With water; bromine; zinc(II) chloride; In tetrachloromethane; ethanol; dichloromethane; chlorobenzene; 1: Friedel Crafts acylation;
DOI:10.1021/jm200505e