2-azidoethyl (5-acetamido-9-(2-benzyl-5-methyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2→3)-β-D-galactopyranosyl-(1→4)-2-acetamido-2-deoxy-β-Dglucopyranoside

Base Information

Chemical Name:2-azidoethyl (5-acetamido-9-(2-benzyl-5-methyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2→3)-β-D-galactopyranosyl-(1→4)-2-acetamido-2-deoxy-β-Dglucopyranoside
CAS No.:1397938-28-1
Molecular Formula:C₄₂H₅₆N₈O₂₀S
Molecular Weight:1025.01
Hs Code.:

2-azidoethyl (5-acetamido-9-(2-benzyl-5-methyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2→3)-β-D-galactopyranosyl-(1→4)-2-acetamido-2-deoxy-β-Dglucopyranoside

Synonyms:2-azidoethyl (5-acetamido-9-(2-benzyl-5-methyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2→3)-β-D-galactopyranosyl-(1→4)-2-acetamido-2-deoxy-β-Dglucopyranoside

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Chemical Property of 2-azidoethyl (5-acetamido-9-(2-benzyl-5-methyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2→3)-β-D-galactopyranosyl-(1→4)-2-acetamido-2-deoxy-β-Dglucopyranoside

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Technology Process of 2-azidoethyl (5-acetamido-9-(2-benzyl-5-methyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2→3)-β-D-galactopyranosyl-(1→4)-2-acetamido-2-deoxy-β-Dglucopyranoside

There total 3 articles about 2-azidoethyl (5-acetamido-9-(2-benzyl-5-methyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2→3)-β-D-galactopyranosyl-(1→4)-2-acetamido-2-deoxy-β-Dglucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1398144-66-5
C₂₇H₄₆N₆O₁₈

: 1397938-48-5
C₁₉H₁₅N₃O₅S

: 1397938-28-1
2-azidoethyl (5-acetamido-9-(2-benzyl-5-methyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2→3)-β-D-galactopyranosyl-(1→4)-2-acetamido-2-deoxy-β-Dglucopyranoside

Guidance literature:: C₂₇H₄₆N₆O₁₈; C₁₉H₁₅N₃O₅S; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; at 20 ℃;

In water;
DOI:10.1021/ja307501e

Reference yield:

: 338971-38-3
2-azidoethyl (β-D-galactopyranosyl)-(1->4)-O-2-acetamido-2-deoxy-β-D-glucopyranoside

: 1397938-28-1
2-azidoethyl (5-acetamido-9-(2-benzyl-5-methyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2→3)-β-D-galactopyranosyl-(1→4)-2-acetamido-2-deoxy-β-Dglucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: pasteurella multocida α2?3-sialyltransferase 1

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran; water / 20 °C

2.2: Amberlite^TM Resin IR-120 H⁺

With pasteurella multocida α2?3-sialyltransferase 1; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water;
DOI:10.1021/ja307501e

Reference yield:

: C₂₀H₃₂N₅O₁₆P

: 1397938-28-1
2-azidoethyl (5-acetamido-9-(2-benzyl-5-methyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2→3)-β-D-galactopyranosyl-(1→4)-2-acetamido-2-deoxy-β-Dglucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: pasteurella multocida α2?3-sialyltransferase 1

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran; water / 20 °C

2.2: Amberlite^TM Resin IR-120 H⁺

With pasteurella multocida α2?3-sialyltransferase 1; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water;
DOI:10.1021/ja307501e