(Z)-N-((2R,3S,4R)-3,4-isopropylidenedioxy-1-(phenylthio)-octadecan-2-yl)tetracos-15-enamide

Base Information

Chemical Name:(Z)-N-((2R,3S,4R)-3,4-isopropylidenedioxy-1-(phenylthio)-octadecan-2-yl)tetracos-15-enamide
CAS No.:1571918-39-2
Molecular Formula:C₅₁H₉₁NO₃S
Molecular Weight:798.354
Hs Code.:

Synonyms:(Z)-N-((2R,3S,4R)-3,4-isopropylidenedioxy-1-(phenylthio)-octadecan-2-yl)tetracos-15-enamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-N-((2R,3S,4R)-3,4-isopropylidenedioxy-1-(phenylthio)-octadecan-2-yl)tetracos-15-enamide

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Technology Process of (Z)-N-((2R,3S,4R)-3,4-isopropylidenedioxy-1-(phenylthio)-octadecan-2-yl)tetracos-15-enamide

There total 2 articles about (Z)-N-((2R,3S,4R)-3,4-isopropylidenedioxy-1-(phenylthio)-octadecan-2-yl)tetracos-15-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 145411-43-4
(Z)-tetracos-15-enoyl chloride

: 1571918-39-2
(Z)-N-((2R,3S,4R)-3,4-isopropylidenedioxy-1-(phenylthio)-octadecan-2-yl)tetracos-15-enamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / -10 - 20 °C / Inert atmosphere

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.05 h / Inert atmosphere

2.2: Sealed tube; Microwave irradiation

With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/jo500061w

Reference yield:

: 506-37-6
Nervonic acid

: 1571918-39-2
(Z)-N-((2R,3S,4R)-3,4-isopropylidenedioxy-1-(phenylthio)-octadecan-2-yl)tetracos-15-enamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / 2 h / Reflux; Inert atmosphere

2.1: triethylamine / dichloromethane / -10 - 20 °C / Inert atmosphere

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.05 h / Inert atmosphere

3.2: Sealed tube; Microwave irradiation

With thionyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/jo500061w

Reference yield: 72.0%

: 1571918-39-2
(Z)-N-((2R,3S,4R)-3,4-isopropylidenedioxy-1-(phenylthio)-octadecan-2-yl)tetracos-15-enamide

: 1571918-40-5
(Z)-N-((2R,3S,4R)-3,4-dihydroxy-1-(phenylthio)octadecan-2-yl)tetracos-15-enamide

Guidance literature:: With [(1S)-7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl]methanesulfonic acid; In methanol; dichloromethane; at 30 ℃; Inert atmosphere;
DOI:10.1021/jo500061w