triphenyllead benzenecarboselenoate

Base Information

Chemical Name:triphenyllead benzenecarboselenoate
CAS No.:128816-51-3
Molecular Formula:C₂₅H₂₀OPbSe
Molecular Weight:622.593
Hs Code.:

Synonyms:triphenyllead benzenecarboselenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenyllead benzenecarboselenoate

Chemical Property:

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Technology Process of triphenyllead benzenecarboselenoate

There total 1 articles about triphenyllead benzenecarboselenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1153-06-6
triphenyllead(IV) chloride

: 128816-63-7
sodium benzenecarboselenoate

: 128816-51-3
triphenyllead benzenecarboselenoate

Guidance literature:: In diethyl ether; byproducts: NaCl; addn. of Ph3PbCl to a suspn. of Na-selenocarboxylate and Ph3PbCl in ether, stirring at 0°C for 1 h (under Ar); filtn. of ppts., evapn. of the solvent under reduced pressure, recrystn. from ether/hexane, elem. anal.;
DOI:10.1016/0022-328X(90)80004-J

Reference yield: 78.0%

: 34837-55-3
Phenylselenyl bromide

: 128816-51-3
triphenyllead benzenecarboselenoate

: 111931-75-0
Se(Se)-phenyl diselenoperbenzoate

Guidance literature:: In diethyl ether; at 20 ℃; for 2h;
DOI:10.1016/0022-328X(90)80004-J

Reference yield: 78.0%

: 128816-51-3
triphenyllead benzenecarboselenoate

: 34837-55-3
Phenylselenyl bromide

: 111931-75-0
Se(Se)-phenyl diselenoperbenzoate

Guidance literature:: In diethyl ether; byproducts: (C6H5)3PbBr; addn. of PhSeBr to a soln. of PhCOSePbPh3 in ether, stirring at 20°C for 2 h (under Ar); evapn. of solvent in vacuo (10°C, 15 torr), addn. of hexane, cooling to -20°C for 40 h, filtn. of ppt. (Ph3PbBr), evapn. of filtrate in vacuo;
DOI:10.1016/0022-328X(90)80004-J