2-(4-carbomethoxyphenylcyclopropane)-1,1-dicarboxylic acid dimethyl ester

Base Information

Chemical Name:2-(4-carbomethoxyphenylcyclopropane)-1,1-dicarboxylic acid dimethyl ester
CAS No.:1034147-67-5
Molecular Formula:C₁₅H₁₆O₆
Molecular Weight:292.288
Hs Code.:

Synonyms:2-(4-carbomethoxyphenylcyclopropane)-1,1-dicarboxylic acid dimethyl ester

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Chemical Property of 2-(4-carbomethoxyphenylcyclopropane)-1,1-dicarboxylic acid dimethyl ester

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Technology Process of 2-(4-carbomethoxyphenylcyclopropane)-1,1-dicarboxylic acid dimethyl ester

There total 2 articles about 2-(4-carbomethoxyphenylcyclopropane)-1,1-dicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1774-47-6
trimethylsulfoxonium iodide

: 104633-19-4
dimethyl 2-[4-(methoxycarbonyl)benzylidene]malonate

: 1034147-67-5
2-(4-carbomethoxyphenylcyclopropane)-1,1-dicarboxylic acid dimethyl ester

Guidance literature:: trimethylsulfoxonium iodide; With sodium hydride; In N,N-dimethyl-formamide; for 0.75h;

dimethyl 2-[4-(methoxycarbonyl)benzylidene]malonate; In N,N-dimethyl-formamide; for 2h; Further stages.;
DOI:10.1021/ja8015928

Reference yield: 44.0%

: 1076-96-6
methyl 4-vinylbenzoate

: 868-26-8
dimethyl 2-bromomalonate

: 1034147-67-5
2-(4-carbomethoxyphenylcyclopropane)-1,1-dicarboxylic acid dimethyl ester

Guidance literature:: With N,N,N',N'',N'''-pentamethyldiethylenetriamine; CuH₁₂O₆⁽²⁺⁾*2BF₄^(1-); In toluene; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1039/c5cc04697a

Reference yield: 93.0%

: 1197-51-9
N-propargylbenzylamine

: 1034147-67-5
2-(4-carbomethoxyphenylcyclopropane)-1,1-dicarboxylic acid dimethyl ester

: 1181823-80-2
C₂₅H₂₇NO₆

Guidance literature:: With bis((1,1,1-trifluoro-N-(trifluoromethyl)sulfonyl)methylsulfonamido)zinc; In benzene; Inert atmosphere; Reflux;
DOI:10.1021/ol901435k