4-(4-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-1,1-bis-{3-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-propyl}-butyl)-phenol

Base Information

Chemical Name:4-(4-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-1,1-bis-{3-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-propyl}-butyl)-phenol
CAS No.:224191-95-1
Molecular Formula:C₆₄H₈₀O₄
Molecular Weight:913.337
Hs Code.:

Synonyms:4-(4-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-1,1-bis-{3-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-propyl}-butyl)-phenol

Suppliers and Price of 4-(4-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-1,1-bis-{3-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-propyl}-butyl)-phenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(4-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-1,1-bis-{3-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-propyl}-butyl)-phenol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-(4-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-1,1-bis-{3-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-propyl}-butyl)-phenol

There total 7 articles about 4-(4-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-1,1-bis-{3-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-propyl}-butyl)-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 224191-80-4
4-triallylmethylphenol

: 224191-94-0
propionic acid 4-[4-iodo-1,1-bis-(3-iodo-propyl)-butyl]-phenyl ester

: 224191-95-1
4-(4-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-1,1-bis-{3-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-propyl}-butyl)-phenol

Guidance literature:: With water; potassium carbonate; In N,N-dimethyl-formamide; at 20 - 40 ℃; for 60h;
DOI:10.1039/B000370K

Reference yield:

: 224191-80-4
4-triallylmethylphenol

: 224191-95-1
4-(4-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-1,1-bis-{3-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-propyl}-butyl)-phenol

Guidance literature:: Multi-step reaction with 5 steps

1.1: 90 percent / KOH / dimethylsulfoxide / 2 h / 20 °C

2.1: BH₃; 2-methyl-2-butene / tetrahydrofuran / -15 °C

2.2: 86 percent / H₂O₂; NaOH / H₂O; tetrahydrofuran / 15 h / 50 °C

3.1: 97 percent / NaI; SiMe₃Cl / acetonitrile / 48 h / 80 °C

4.1: 94 percent / diisopropylethylamine / CH₂Cl₂ / 16 h

5.1: 30 percent / K₂CO₃; H₂O / dimethylformamide / 60 h / 20 - 40 °C

With potassium hydroxide; chloro-trimethyl-silane; 2-methyl-but-2-ene; borane; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; sodium iodide; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; 2.1: hydroboration (Brown);
DOI:10.1039/B000370K

Reference yield:

: 224191-93-9
p-[1,1-di(3-iodopropyl)-4-iodobutyl]phenol

: 224191-95-1
4-(4-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-1,1-bis-{3-[4-(1,1-diallyl-but-3-enyl)-phenoxy]-propyl}-butyl)-phenol

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / diisopropylethylamine / CH₂Cl₂ / 16 h

2: 30 percent / K₂CO₃; H₂O / dimethylformamide / 60 h / 20 - 40 °C

With water; potassium carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/B000370K