N,N'-bis(4-n-butylphenyl)-N,N'-bis{4-[3-(triethoxysilyl)propyl]carbamoyloxymethylphenyl}-1,1'-biphenyl-4,4'-diamine

Base Information

Chemical Name:N,N'-bis(4-n-butylphenyl)-N,N'-bis{4-[3-(triethoxysilyl)propyl]carbamoyloxymethylphenyl}-1,1'-biphenyl-4,4'-diamine
CAS No.:1262958-12-2
Molecular Formula:C₆₆H₉₀N₄O₁₀Si₂
Molecular Weight:1155.63
Hs Code.:

Synonyms:N,N'-bis(4-n-butylphenyl)-N,N'-bis{4-[3-(triethoxysilyl)propyl]carbamoyloxymethylphenyl}-1,1'-biphenyl-4,4'-diamine

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Chemical Property of N,N'-bis(4-n-butylphenyl)-N,N'-bis{4-[3-(triethoxysilyl)propyl]carbamoyloxymethylphenyl}-1,1'-biphenyl-4,4'-diamine

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Technology Process of N,N'-bis(4-n-butylphenyl)-N,N'-bis{4-[3-(triethoxysilyl)propyl]carbamoyloxymethylphenyl}-1,1'-biphenyl-4,4'-diamine

There total 6 articles about N,N'-bis(4-n-butylphenyl)-N,N'-bis{4-[3-(triethoxysilyl)propyl]carbamoyloxymethylphenyl}-1,1'-biphenyl-4,4'-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.6%

: 1262958-14-4
N,N'-bis(4-n-butylphenyl)-N,N'-bis(4-hydroxymethylphen-yl)-1,1'-biphenyl-4,4'-diamine

: 24801-88-5
3-(triethoxypropyl) isocyanate

: 1262958-12-2
N,N'-bis(4-n-butylphenyl)-N,N'-bis{4-[3-(triethoxysilyl)propyl]carbamoyloxymethylphenyl}-1,1'-biphenyl-4,4'-diamine

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 70 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja1061517

Reference yield:

: 216168-75-1
N,N'-bis(p-formylphenyl)-N,N'-bis(4-n-butylphenyl)biphenyl-4,4'-diamine

: 1262958-12-2
N,N'-bis(4-n-butylphenyl)-N,N'-bis{4-[3-(triethoxysilyl)propyl]carbamoyloxymethylphenyl}-1,1'-biphenyl-4,4'-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; sodium hydroxide / tetrahydrofuran; ethanol / 1 h / 0 - 20 °C / Inert atmosphere

2: triethylamine / N,N-dimethyl-formamide / 12 h / 70 °C / Inert atmosphere

With sodium tetrahydroborate; triethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja1061517

Reference yield:

: 92-86-4
4-(4-bromophenyl)bromobenzene

: 1262958-12-2
N,N'-bis(4-n-butylphenyl)-N,N'-bis{4-[3-(triethoxysilyl)propyl]carbamoyloxymethylphenyl}-1,1'-biphenyl-4,4'-diamine

Guidance literature:: Multi-step reaction with 5 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis-(diphenylphosphino)ferrocene; sodium t-butanolate / toluene / 24 h / 80 °C / Inert atmosphere

2: toluene / 36 h / 100 °C / Inert atmosphere

3: trichlorophosphate / 1,2-dichloro-ethane / 0 - 90 °C / Inert atmosphere

4: sodium tetrahydroborate; sodium hydroxide / tetrahydrofuran; ethanol / 1 h / 0 - 20 °C / Inert atmosphere

5: triethylamine / N,N-dimethyl-formamide / 12 h / 70 °C / Inert atmosphere

With 1,1'-bis-(diphenylphosphino)ferrocene; sodium tetrahydroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triethylamine; sodium hydroxide; sodium t-butanolate; trichlorophosphate; In tetrahydrofuran; ethanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja1061517