(3Z)-1,6-anhydro-4-O-(tert-butyldiphenylsilyl)-2-O-(1'-ethoxy-2'-iodoethyl)-3-deoxy-3-methoxyimine-β-D-arabino-hexopyranose

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Chemical Name:(3Z)-1,6-anhydro-4-O-(tert-butyldiphenylsilyl)-2-O-(1'-ethoxy-2'-iodoethyl)-3-deoxy-3-methoxyimine-β-D-arabino-hexopyranose
CAS No.:190188-91-1
Molecular Formula:C₂₇H₃₆INO₆Si
Molecular Weight:625.576
Hs Code.:

Synonyms:(3Z)-1,6-anhydro-4-O-(tert-butyldiphenylsilyl)-2-O-(1'-ethoxy-2'-iodoethyl)-3-deoxy-3-methoxyimine-β-D-arabino-hexopyranose

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Chemical Property of (3Z)-1,6-anhydro-4-O-(tert-butyldiphenylsilyl)-2-O-(1'-ethoxy-2'-iodoethyl)-3-deoxy-3-methoxyimine-β-D-arabino-hexopyranose

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Technology Process of (3Z)-1,6-anhydro-4-O-(tert-butyldiphenylsilyl)-2-O-(1'-ethoxy-2'-iodoethyl)-3-deoxy-3-methoxyimine-β-D-arabino-hexopyranose

There total 6 articles about (3Z)-1,6-anhydro-4-O-(tert-butyldiphenylsilyl)-2-O-(1'-ethoxy-2'-iodoethyl)-3-deoxy-3-methoxyimine-β-D-arabino-hexopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 109-92-2,25104-37-4
ethyl vinyl ether

: 190188-88-6
(3Z)-1,6-anhydro-4-O-(tert-butyldiphenylsilyl)-3-deoxy-3-methoxyimine-β-D-arabino-hexopyranose

: 190188-91-1
(3Z)-1,6-anhydro-4-O-(tert-butyldiphenylsilyl)-2-O-(1'-ethoxy-2'-iodoethyl)-3-deoxy-3-methoxyimine-β-D-arabino-hexopyranose

Guidance literature:: With N-iodo-succinimide; In tetrahydrofuran; -20 deg C --> room temp.;
DOI:10.1016/S0040-4039(97)00460-7

Reference yield:

: 14440-51-8
1,6-anhydro-2,3-O-isopropylidene-β-D-mannopyranose

: 190188-91-1
(3Z)-1,6-anhydro-4-O-(tert-butyldiphenylsilyl)-2-O-(1'-ethoxy-2'-iodoethyl)-3-deoxy-3-methoxyimine-β-D-arabino-hexopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / imidazole / dimethylformamide

3: 84 percent / pyridine / CH₂Cl₂

4: 90 percent / N-iodosuccinimide / tetrahydrofuran / -20 deg C --> room temp.

With pyridine; 1H-imidazole; N-iodo-succinimide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(97)00460-7

Reference yield:

: 149793-78-2
1,6-anhydro-4-O-(tert-butyldiphenylsilyl)-β-D-arabino-hexopyran-3-ulose

: 190188-91-1
(3Z)-1,6-anhydro-4-O-(tert-butyldiphenylsilyl)-2-O-(1'-ethoxy-2'-iodoethyl)-3-deoxy-3-methoxyimine-β-D-arabino-hexopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / pyridine / CH₂Cl₂

2: 90 percent / N-iodosuccinimide / tetrahydrofuran / -20 deg C --> room temp.

With pyridine; N-iodo-succinimide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(97)00460-7