(3R,4S,5S,6R)-6-[(N-benzyl-N-(benzyloxycarbonyl))amino]-3,5-bis(benzyloxy)-4-fluoro-1,8-nonadiene

Base Information

Chemical Name:(3R,4S,5S,6R)-6-[(N-benzyl-N-(benzyloxycarbonyl))amino]-3,5-bis(benzyloxy)-4-fluoro-1,8-nonadiene
CAS No.:1236278-83-3
Molecular Formula:C₃₈H₄₀FNO₄
Molecular Weight:593.738
Hs Code.:

Synonyms:(3R,4S,5S,6R)-6-[(N-benzyl-N-(benzyloxycarbonyl))amino]-3,5-bis(benzyloxy)-4-fluoro-1,8-nonadiene

Suppliers and Price of (3R,4S,5S,6R)-6-[(N-benzyl-N-(benzyloxycarbonyl))amino]-3,5-bis(benzyloxy)-4-fluoro-1,8-nonadiene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (3R,4S,5S,6R)-6-[(N-benzyl-N-(benzyloxycarbonyl))amino]-3,5-bis(benzyloxy)-4-fluoro-1,8-nonadiene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3R,4S,5S,6R)-6-[(N-benzyl-N-(benzyloxycarbonyl))amino]-3,5-bis(benzyloxy)-4-fluoro-1,8-nonadiene

There total 10 articles about (3R,4S,5S,6R)-6-[(N-benzyl-N-(benzyloxycarbonyl))amino]-3,5-bis(benzyloxy)-4-fluoro-1,8-nonadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.6%

: 1236278-81-1
(3R,4S,5S,6R)-6-[(N-benzyl)amino]-3,5-bis(benzyloxy)-4-fluoro-1,8-nonadiene

: 501-53-1,94274-21-2
benzyl chloroformate

: 1236278-83-3
(3R,4S,5S,6R)-6-[(N-benzyl-N-(benzyloxycarbonyl))amino]-3,5-bis(benzyloxy)-4-fluoro-1,8-nonadiene

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; at 25 ℃; for 14h;
DOI:10.1515/znb-2010-0402

Reference yield:

: 100-46-9
benzylamine

: 1236278-83-3
(3R,4S,5S,6R)-6-[(N-benzyl-N-(benzyloxycarbonyl))amino]-3,5-bis(benzyloxy)-4-fluoro-1,8-nonadiene

Guidance literature:: Multi-step reaction with 2 steps

1: zinc

2: sodium hydrogencarbonate / dichloromethane / 14 h / 25 °C

With sodium hydrogencarbonate; zinc; In dichloromethane;
DOI:10.1515/znb-2010-0402

Reference yield:

: C₄₀H₃₉FO₅

: 1236278-83-3
(3R,4S,5S,6R)-6-[(N-benzyl-N-(benzyloxycarbonyl))amino]-3,5-bis(benzyloxy)-4-fluoro-1,8-nonadiene

Guidance literature:: Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid / methanol; dichloromethane / 24 h / 25 °C

2: 1H-imidazole; iodine; triphenylphosphine / toluene / 2 h / 95 °C

3: zinc

4: sodium hydrogencarbonate / dichloromethane / 14 h / 25 °C

With 1H-imidazole; iodine; sodium hydrogencarbonate; toluene-4-sulfonic acid; triphenylphosphine; zinc; In methanol; dichloromethane; toluene;
DOI:10.1515/znb-2010-0402