(4aR,4bS,6aS,7S,9aS,9bS)-4a,6a-dimethyl-2-oxohexadecahydro-1H-indeno[5,4-f]quinoline-7-carboxylic acid

Base Information

Chemical Name:(4aR,4bS,6aS,7S,9aS,9bS)-4a,6a-dimethyl-2-oxohexadecahydro-1H-indeno[5,4-f]quinoline-7-carboxylic acid
CAS No.:161511-08-6
Molecular Formula:C₁₉H₂₉NO₃
Molecular Weight:319.444
Hs Code.:

Synonyms:(4aR,4bS,6aS,7S,9aS,9bS)-4a,6a-dimethyl-2-oxohexadecahydro-1H-indeno[5,4-f]quinoline-7-carboxylic acid

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Chemical Property of (4aR,4bS,6aS,7S,9aS,9bS)-4a,6a-dimethyl-2-oxohexadecahydro-1H-indeno[5,4-f]quinoline-7-carboxylic acid

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Technology Process of (4aR,4bS,6aS,7S,9aS,9bS)-4a,6a-dimethyl-2-oxohexadecahydro-1H-indeno[5,4-f]quinoline-7-carboxylic acid

There total 2 articles about (4aR,4bS,6aS,7S,9aS,9bS)-4a,6a-dimethyl-2-oxohexadecahydro-1H-indeno[5,4-f]quinoline-7-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.2%

: 103335-54-2
(4aR,4bS,6aS,7S,9aS,9bS)-4a,6a-dimethyl-2-oxo-2,3,4,4a,4b,5,6,6a,7,8,9,9a,9b,10-tetradecahydro-1H-indeno[5,4-f]quinoline-7-carboxylic acid

: 161511-08-6,1430804-94-6
(4aR,4bS,6aS,7S,9aS,9bS)-4a,6a-dimethyl-2-oxohexadecahydro-1H-indeno[5,4-f]quinoline-7-carboxylic acid

Guidance literature:: With 3% Pd/C; hydrogen; sodium hydroxide; In water; at 38 ℃; for 12h; under 225.023 Torr; Pressure; Reagent/catalyst; Temperature; Inert atmosphere; Large scale;

Reference yield:

: 302-97-6
androst-4-en-3-one-17β-carboxylic acid

: 161511-08-6,1430804-94-6
(4aR,4bS,6aS,7S,9aS,9bS)-4a,6a-dimethyl-2-oxohexadecahydro-1H-indeno[5,4-f]quinoline-7-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium periodate; potassium permanganate; potassium carbonate / tert-butyl alcohol / 1 h / 40 °C

2: ammonia / ethylene glycol / 120 - 140 °C

3: hydrogenchloride; sodium cyanoborohydride / methanol; water / pH 2

With hydrogenchloride; potassium permanganate; sodium periodate; ammonia; sodium cyanoborohydride; potassium carbonate; In methanol; water; ethylene glycol; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2011.03.102