5-{amino[1-(benzo[d][1,3]dioxol-5-yl)-1H-tetrazol-5-yl]methyl}-2-methoxyphenol

Base Information

Chemical Name:5-{amino[1-(benzo[d][1,3]dioxol-5-yl)-1H-tetrazol-5-yl]methyl}-2-methoxyphenol
CAS No.:1268445-64-2
Molecular Formula:C₁₆H₁₅N₅O₄
Molecular Weight:341.326
Hs Code.:

Synonyms:5-{amino[1-(benzo[d][1,3]dioxol-5-yl)-1H-tetrazol-5-yl]methyl}-2-methoxyphenol

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Chemical Property of 5-{amino[1-(benzo[d][1,3]dioxol-5-yl)-1H-tetrazol-5-yl]methyl}-2-methoxyphenol

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Technology Process of 5-{amino[1-(benzo[d][1,3]dioxol-5-yl)-1H-tetrazol-5-yl]methyl}-2-methoxyphenol

There total 4 articles about 5-{amino[1-(benzo[d][1,3]dioxol-5-yl)-1H-tetrazol-5-yl]methyl}-2-methoxyphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1268445-53-9
5-{[1-(benzo[d][1,3]dioxol-5-yl)-1H-tetrazol-5-yl](benzylamino)methyl}-2-methoxyphenol

: 1268445-64-2
5-{amino[1-(benzo[d][1,3]dioxol-5-yl)-1H-tetrazol-5-yl]methyl}-2-methoxyphenol

Guidance literature:: With 10% palladium on activated carbon; hydrogen; In methanol; at 60 ℃; for 24h;
DOI:10.1055/s-0030-1258273

Reference yield:

: 621-59-0
isovanillin

: 1268445-64-2
5-{amino[1-(benzo[d][1,3]dioxol-5-yl)-1H-tetrazol-5-yl]methyl}-2-methoxyphenol

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilylazide / methanol / 72 h / 20 °C / Inert atmosphere

2: 10% palladium on activated carbon; hydrogen / methanol / 24 h / 60 °C

With trimethylsilylazide; 10% palladium on activated carbon; hydrogen; In methanol; 1: Ugi like four component reaction;
DOI:10.1055/s-0030-1258273

Reference yield:

: 165459-70-1
3,4-(methylenedioxy)benzeneisonitrile

: 1268445-64-2
5-{amino[1-(benzo[d][1,3]dioxol-5-yl)-1H-tetrazol-5-yl]methyl}-2-methoxyphenol

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilylazide / methanol / 72 h / 20 °C / Inert atmosphere

2: 10% palladium on activated carbon; hydrogen / methanol / 24 h / 60 °C

With trimethylsilylazide; 10% palladium on activated carbon; hydrogen; In methanol; 1: Ugi like four component reaction;
DOI:10.1055/s-0030-1258273