2,4,6-Trimethyl-benzenesulfonate2-amino-1-methyl-3,4-dihydro-pyrazino[1,2-a]indol-2-ium;

Base Information

• Chemical Name: 2,4,6-Trimethyl-benzenesulfonate2-amino-1-methyl-3,4-dihydro-pyrazino[1,2-a]indol-2-ium
• CAS No.: 138747-18-9
• Molecular Formula: C₉H₁₁O₃S*C₁₂H₁₄N₃
• Molecular Weight: 399.514

Synonyms:2,4,6-Trimethyl-benzenesulfonate2-amino-1-methyl-3,4-dihydro-pyrazino[1,2-a]indol-2-ium;

Chemical Property of 2,4,6-Trimethyl-benzenesulfonate2-amino-1-methyl-3,4-dihydro-pyrazino[1,2-a]indol-2-ium;

Chemical Property:

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Technology Process of 2,4,6-Trimethyl-benzenesulfonate2-amino-1-methyl-3,4-dihydro-pyrazino[1,2-a]indol-2-ium;

There total 2 articles about 2,4,6-Trimethyl-benzenesulfonate2-amino-1-methyl-3,4-dihydro-pyrazino[1,2-a]indol-2-ium; which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

1-Methyl-3,4-dihydropyrazino<1,2-a>indole → 2,4,6-Trimethyl-benzenesulfonate2-amino-1-methyl-3,4-dihydro-pyrazino[1,2-a]indol-2-ium; (138747-18-9)

Guidance literature:

With mesitylenesulfonylhydroxylamine; In dichloromethane; for 0.166667h; Ambient temperature;

DOI:10.1016/S0040-4020(01)89735-0

Reference yield:

N-<2-(indol-1-yl)ethyl>acetamide (56903-24-3) → 2,4,6-Trimethyl-benzenesulfonate2-amino-1-methyl-3,4-dihydro-pyrazino[1,2-a]indol-2-ium; (138747-18-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 50 percent / POCl₃ / 1 h / Heating

2: 50 percent / O-hydroxylaminomesitylenesulfonate / CH₂Cl₂ / 0.17 h / Ambient temperature

With mesitylenesulfonylhydroxylamine; trichlorophosphate; In dichloromethane;

DOI:10.1016/S0040-4020(01)89735-0

Reference yield: 71.0%

2,4,6-Trimethyl-benzenesulfonate2-amino-1-methyl-3,4-dihydro-pyrazino[1,2-a]indol-2-ium; (138747-18-9) + 9,10-phenanthrenequinone (84-11-7) → C26H18N3(1+)*C9H11O3S(1-) (138767-00-7)

Guidance literature:

With sodium acetate; In acetone; for 1h; Heating;

DOI:10.1016/S0040-4020(01)89735-0

upstream raw materials:

N-<2-(indol-1-yl)ethyl>acetamide

Downstream raw materials:

C₂₆H₁₈N₃⁽¹⁺⁾*C₉H₁₁O₃S^(1-)

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