di-tert-butyl(((1,4-phenylenebis(methylene))bis(azanediyl))bis(butane-4,1-diyl))bis((4-((tert-butoxycarbonyl)(methyl)amino)butyl)carbamate),

Base Information

Chemical Name:di-tert-butyl(((1,4-phenylenebis(methylene))bis(azanediyl))bis(butane-4,1-diyl))bis((4-((tert-butoxycarbonyl)(methyl)amino)butyl)carbamate),
CAS No.:1446751-84-3
Molecular Formula:C₄₆H₈₄N₆O₈
Molecular Weight:849.208
Hs Code.:

Synonyms:di-tert-butyl(((1,4-phenylenebis(methylene))bis(azanediyl))bis(butane-4,1-diyl))bis((4-((tert-butoxycarbonyl)(methyl)amino)butyl)carbamate),

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Chemical Property of di-tert-butyl(((1,4-phenylenebis(methylene))bis(azanediyl))bis(butane-4,1-diyl))bis((4-((tert-butoxycarbonyl)(methyl)amino)butyl)carbamate),

Chemical Property:

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Technology Process of di-tert-butyl(((1,4-phenylenebis(methylene))bis(azanediyl))bis(butane-4,1-diyl))bis((4-((tert-butoxycarbonyl)(methyl)amino)butyl)carbamate),

There total 10 articles about di-tert-butyl(((1,4-phenylenebis(methylene))bis(azanediyl))bis(butane-4,1-diyl))bis((4-((tert-butoxycarbonyl)(methyl)amino)butyl)carbamate), which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1446751-84-3
di-tert-butyl(((1,4-phenylenebis(methylene))bis(azanediyl))bis(butane-4,1-diyl))bis((4-((tert-butoxycarbonyl)(methyl)amino)butyl)carbamate),

Guidance literature:: In methanol; dichloromethane; at 20 ℃; Inert atmosphere;

With sodium tetrahydroborate; In methanol; dichloromethane; at 0 - 20 ℃; for 2h;

Reference yield:

: C₄₆H₈₀N₆O₈

: 1446751-84-3
di-tert-butyl(((1,4-phenylenebis(methylene))bis(azanediyl))bis(butane-4,1-diyl))bis((4-((tert-butoxycarbonyl)(methyl)amino)butyl)carbamate),

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jm400496a

Reference yield:

: 99207-32-6
4-(N-tert-Butyloxycarbonyl-N-methylamino)butanol

: 1446751-84-3
di-tert-butyl(((1,4-phenylenebis(methylene))bis(azanediyl))bis(butane-4,1-diyl))bis((4-((tert-butoxycarbonyl)(methyl)amino)butyl)carbamate),

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / acetonitrile / 1 h / Inert atmosphere; Reflux

3: sodium sulfate / methanol; dichloromethane / 1.08 h / 20 °C / Inert atmosphere

4: methanol; dichloromethane / 0.75 h / 20 °C / Inert atmosphere

5: hydrogenchloride / ethanol; water / 2 h / 0 - 20 °C / Inert atmosphere

6: methanol; dichloromethane / 20 °C / Inert atmosphere

7: sodium tetrahydroborate / methanol; dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; sodium tetrahydroborate; potassium carbonate; sodium sulfate; triethylamine; In methanol; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1021/jm400496a