C₂₈H₂₃FN₂O₇

Base Information

Chemical Name:C₂₈H₂₃FN₂O₇
CAS No.:1206529-41-0
Molecular Formula:C₂₈H₂₃FN₂O₇
Molecular Weight:518.498
Hs Code.:

C<sub>28</sub>H<sub>23</sub>FN<sub>2</sub>O<sub>7</sub>

Synonyms:C₂₈H₂₃FN₂O₇

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Chemical Property of C₂₈H₂₃FN₂O₇

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Technology Process of C₂₈H₂₃FN₂O₇

There total 9 articles about C₂₈H₂₃FN₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1206529-40-9
C₂₈H₂₅FN₂O₆

: 1206529-41-0
C₂₈H₂₃FN₂O₇

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; In water; 1,2-dichloro-ethane; at 20 ℃;

Reference yield:

: 1206529-31-8
C₂₇H₃₄BrFN₂O₆

: 1206529-41-0
C₂₈H₂₃FN₂O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: 3 h / 180 °C

2.1: 2,6-dimethylpyridine; ethyl chlorocarbonylacetate / 1,2-dichloro-ethane / 1.17 h / 20 °C

3.1: sodium ethanolate / ethanol / 1 h / 20 °C

4.1: silver(l) oxide / dichloromethane / 0.33 h / 20 °C

4.2: 20 °C

5.1: acetic acid / water / 20 °C

6.1: dmap; 1H-imidazole / dichloromethane / 20 °C

7.1: sodium hexamethyldisilazane / N,N-dimethyl-formamide / 0.25 h / -40 °C

8.1: trifluoroacetic acid / water; tetrahydrofuran / 20 °C

9.1: 2,2,6,6-tetramethyl-piperidine-N-oxyl / water; 1,2-dichloro-ethane / 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium ethanolate; sodium hexamethyldisilazane; acetic acid; ethyl chlorocarbonylacetate; trifluoroacetic acid; silver(l) oxide; In tetrahydrofuran; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 1206529-36-3
C₂₈H₂₆BrFN₂O₆

: 1206529-41-0
C₂₈H₂₃FN₂O₇

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; 1H-imidazole / dichloromethane / 20 °C

2: sodium hexamethyldisilazane / N,N-dimethyl-formamide / 0.25 h / -40 °C

3: trifluoroacetic acid / water; tetrahydrofuran / 20 °C

4: 2,2,6,6-tetramethyl-piperidine-N-oxyl / water; 1,2-dichloro-ethane / 20 °C

With 1H-imidazole; dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hexamethyldisilazane; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;