2-(4-isopropyl-3-tetrazol-1-yl-phenylamino)-4-(2,2,6,6-tetramethyl-piperidin-4-ylamino)-pyrimidine-5-carboxylic acid amide

Base Information

Chemical Name:2-(4-isopropyl-3-tetrazol-1-yl-phenylamino)-4-(2,2,6,6-tetramethyl-piperidin-4-ylamino)-pyrimidine-5-carboxylic acid amide
CAS No.:1356493-41-8
Molecular Formula:C₂₄H₃₄N₁₀O
Molecular Weight:478.6
Hs Code.:

Synonyms:2-(4-isopropyl-3-tetrazol-1-yl-phenylamino)-4-(2,2,6,6-tetramethyl-piperidin-4-ylamino)-pyrimidine-5-carboxylic acid amide

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Chemical Property of 2-(4-isopropyl-3-tetrazol-1-yl-phenylamino)-4-(2,2,6,6-tetramethyl-piperidin-4-ylamino)-pyrimidine-5-carboxylic acid amide

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Technology Process of 2-(4-isopropyl-3-tetrazol-1-yl-phenylamino)-4-(2,2,6,6-tetramethyl-piperidin-4-ylamino)-pyrimidine-5-carboxylic acid amide

There total 7 articles about 2-(4-isopropyl-3-tetrazol-1-yl-phenylamino)-4-(2,2,6,6-tetramethyl-piperidin-4-ylamino)-pyrimidine-5-carboxylic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1309831-10-4
5-aminocarbonyl-2-chloro-N₄-(2,2,6,6-tetramethylpiperidin-4-yl)-4-pyrimidineamine

: 1356493-66-7
4-isopropyl-3-(1H-tetrazol-1-yl)benzenamine

: 1356493-41-8
2-(4-isopropyl-3-tetrazol-1-yl-phenylamino)-4-(2,2,6,6-tetramethyl-piperidin-4-ylamino)-pyrimidine-5-carboxylic acid amide

Guidance literature:: 5-aminocarbonyl-2-chloro-N₄-(2,2,6,6-tetramethylpiperidin-4-yl)-4-pyrimidineamine; 4-isopropyl-3-(1H-tetrazol-1-yl)benzenamine; With toluene-4-sulfonic acid; In isopropyl alcohol; at 100 ℃; for 3h;

With sodium hydroxide; In isopropyl alcohol;

Reference yield:

: 643-28-7
2-isopropylaniline

: 1356493-41-8
2-(4-isopropyl-3-tetrazol-1-yl-phenylamino)-4-(2,2,6,6-tetramethyl-piperidin-4-ylamino)-pyrimidine-5-carboxylic acid amide

Guidance literature:: Multi-step reaction with 4 steps

1.1: nitric acid; sulfuric acid / 0 °C

2.1: acetic acid / 0.17 h / 20 °C

2.2: 1 h / 120 °C

2.3: 0 °C

3.1: ammonium chloride / iron / ethanol; water / 2 h / Reflux

4.1: toluene-4-sulfonic acid / isopropyl alcohol / 3 h / 100 °C

With sulfuric acid; nitric acid; ammonium chloride; toluene-4-sulfonic acid; acetic acid; iron; In ethanol; water; isopropyl alcohol;

Reference yield:

: 132475-93-5
2-isopropyl-5-nitroaniline

: 1356493-41-8
2-(4-isopropyl-3-tetrazol-1-yl-phenylamino)-4-(2,2,6,6-tetramethyl-piperidin-4-ylamino)-pyrimidine-5-carboxylic acid amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / 0.17 h / 20 °C

1.2: 1 h / 120 °C

1.3: 0 °C

2.1: ammonium chloride / iron / ethanol; water / 2 h / Reflux

3.1: toluene-4-sulfonic acid / isopropyl alcohol / 3 h / 100 °C

With ammonium chloride; toluene-4-sulfonic acid; acetic acid; iron; In ethanol; water; isopropyl alcohol;