4,5-dichloro-2-[[1-[(2E)-3-(4-chlorophenyl)-2-propen-1-yl]-3-azetidinyl]oxy]benzenamine

Base Information

Chemical Name:4,5-dichloro-2-[[1-[(2E)-3-(4-chlorophenyl)-2-propen-1-yl]-3-azetidinyl]oxy]benzenamine
CAS No.:1355345-59-3
Molecular Formula:C₁₈H₁₇Cl₃N₂O
Molecular Weight:383.705
Hs Code.:

Synonyms:4,5-dichloro-2-[[1-[(2E)-3-(4-chlorophenyl)-2-propen-1-yl]-3-azetidinyl]oxy]benzenamine

Suppliers and Price of 4,5-dichloro-2-[[1-[(2E)-3-(4-chlorophenyl)-2-propen-1-yl]-3-azetidinyl]oxy]benzenamine

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Chemical Property of 4,5-dichloro-2-[[1-[(2E)-3-(4-chlorophenyl)-2-propen-1-yl]-3-azetidinyl]oxy]benzenamine

Chemical Property:

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Technology Process of 4,5-dichloro-2-[[1-[(2E)-3-(4-chlorophenyl)-2-propen-1-yl]-3-azetidinyl]oxy]benzenamine

There total 3 articles about 4,5-dichloro-2-[[1-[(2E)-3-(4-chlorophenyl)-2-propen-1-yl]-3-azetidinyl]oxy]benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1355345-58-2
1-[(2E)-3-(4-chlorophenyl)-2-propen-1-yl]-3-(4,5-dichloro-2-nitrophenoxy)azetidine

: 1355345-59-3
4,5-dichloro-2-[[1-[(2E)-3-(4-chlorophenyl)-2-propen-1-yl]-3-azetidinyl]oxy]benzenamine

Guidance literature:: With ammonium chloride; iron; In ethanol; water; for 0.5h; Reflux;

Reference yield:

: 1355345-57-1
1-[(2E)-3-(4-chlorophenyl)-2-propen-1-yl]-3-azetidinol

: 1355345-59-3
4,5-dichloro-2-[[1-[(2E)-3-(4-chlorophenyl)-2-propen-1-yl]-3-azetidinyl]oxy]benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.08 h / 20 °C

1.2: 20 °C

2.1: ammonium chloride / iron / ethanol; water / 0.5 h / Reflux

With sodium hydride; ammonium chloride; iron; In ethanol; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 60691-88-5
(E)-3-(4-chlorophenyl)prop-2-en-1-amine

: 1355345-59-3
4,5-dichloro-2-[[1-[(2E)-3-(4-chlorophenyl)-2-propen-1-yl]-3-azetidinyl]oxy]benzenamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: isopropyl alcohol / 20 °C

1.2: 2.5 h / Reflux

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.08 h / 20 °C

2.2: 20 °C

3.1: ammonium chloride / iron / ethanol; water / 0.5 h / Reflux

With sodium hydride; ammonium chloride; iron; In ethanol; water; N,N-dimethyl-formamide; isopropyl alcohol; mineral oil;