C₃₀H₃₃N₃O₁₂S₃

Base Information

• Chemical Name: C₃₀H₃₃N₃O₁₂S₃
• CAS No.: 110654-55-2
• Molecular Formula: C₃₀H₃₃N₃O₁₂S₃
• Molecular Weight: 723.803
• Mol file: 110654-55-2.mol

Synonyms:C₃₀H₃₃N₃O₁₂S₃

Chemical Property of C₃₀H₃₃N₃O₁₂S₃

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₃₀H₃₃N₃O₁₂S₃

There total 5 articles about C₃₀H₃₃N₃O₁₂S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

1,3,5-Trioxan (110-88-3) + methyl 4-(sulfamoylmethyl)benzoate (110654-40-5) → C30H33N3O12S3 (110654-55-2)

Guidance literature:

With methanesulfonic acid; acetic anhydride; In 1,2-dichloro-ethane; at 35 ℃; for 4h;

DOI:10.1002/jhet.5570230620

Reference yield:

p-Chlorocarbonylbenzylsulphonyl chloride → C30H33N3O12S3 (110654-55-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 47 percent / aq. NH₃ / benzene; CHCl₃

2: 96 percent / 3N aq. NaOH / 24 h / 80 °C

3: conc.H₂SO₄ / 24 h / 65 °C

4: 77 percent / Methanesulphonic acid, acetic anhydride / 1,2-dichloro-ethane / 4 h / 35 °C

With ammonium hydroxide; sodium hydroxide; methanesulfonic acid; sulfuric acid; acetic anhydride; In chloroform; 1,2-dichloro-ethane; benzene;

DOI:10.1002/jhet.5570230620

Reference yield:

4-Sulfamoylmethyl-benzamide (110654-65-4) → C30H33N3O12S3 (110654-55-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 96 percent / 3N aq. NaOH / 24 h / 80 °C

2: conc.H₂SO₄ / 24 h / 65 °C

3: 77 percent / Methanesulphonic acid, acetic anhydride / 1,2-dichloro-ethane / 4 h / 35 °C

With sodium hydroxide; methanesulfonic acid; sulfuric acid; acetic anhydride; In 1,2-dichloro-ethane;

DOI:10.1002/jhet.5570230620

upstream raw materials:

1,3,5-Trioxan

methyl 4-(sulfamoylmethyl)benzoate

4-Sulfamoylmethyl-benzamide

4-Sulfamoylmethyl-benzoic acid