Dimethyl-{4-[4-methyl-5-methylsulfanyl-[1,3]dithiol-(2E)-ylidenemethyl]-phenyl}-amine

Base Information

Chemical Name:Dimethyl-{4-[4-methyl-5-methylsulfanyl-[1,3]dithiol-(2E)-ylidenemethyl]-phenyl}-amine
CAS No.:163226-72-0
Molecular Formula:C₁₄H₁₇NS₃
Molecular Weight:295.494
Hs Code.:

Synonyms:Dimethyl-{4-[4-methyl-5-methylsulfanyl-[1,3]dithiol-(2E)-ylidenemethyl]-phenyl}-amine

Suppliers and Price of Dimethyl-{4-[4-methyl-5-methylsulfanyl-[1,3]dithiol-(2E)-ylidenemethyl]-phenyl}-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Dimethyl-{4-[4-methyl-5-methylsulfanyl-[1,3]dithiol-(2E)-ylidenemethyl]-phenyl}-amine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Dimethyl-{4-[4-methyl-5-methylsulfanyl-[1,3]dithiol-(2E)-ylidenemethyl]-phenyl}-amine

There total 1 articles about Dimethyl-{4-[4-methyl-5-methylsulfanyl-[1,3]dithiol-(2E)-ylidenemethyl]-phenyl}-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 100-10-7
4-dimethylamino-benzaldehyde

: (4-Methyl-5-methylsulfanyl-[1,3]dithiol-2-yl)-phosphonic acid diethyl ester

: Dimethyl-{4-[4-methyl-5-methylsulfanyl-[1,3]dithiol-(2Z)-ylidenemethyl]-phenyl}-amine

: 163226-72-0
Dimethyl-{4-[4-methyl-5-methylsulfanyl-[1,3]dithiol-(2E)-ylidenemethyl]-phenyl}-amine

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; 1.) -78 deg C, 10 min, 2.) r.t., 2 h;
DOI:10.1021/jo00113a026

Reference yield: 73.0%

: 163226-72-0
Dimethyl-{4-[4-methyl-5-methylsulfanyl-[1,3]dithiol-(2E)-ylidenemethyl]-phenyl}-amine

: C₂₈H₃₂N₂S₆

Guidance literature:: In acetonitrile; electrolysis: platinum grid as a working electrode, 1 M tetrabutylammonium hexafluorophosphate as the supporting electrolyte, 0.6-0.8 V then -0.2 V;
DOI:10.1021/jo00113a026

Reference yield:

: 163226-72-0
Dimethyl-{4-[4-methyl-5-methylsulfanyl-[1,3]dithiol-(2E)-ylidenemethyl]-phenyl}-amine

: C₂₈H₃₄N₂S₆⁽²⁺⁾

Guidance literature:: With 2,6-dimethylpyridine; In acetonitrile; at 20 ℃; Rate constant; cyclic voltammetry: Pt wire as a counter electrode, aqueous saturated calomel electrode as a reference electrode, NEt₄BF₄ as a supporting electrolyte;
DOI:10.1021/jp961048v