(1S,2S,5R)-2-hydroxy-N,N,2-trimethyl-5-(prop-1-en-2-yl)cyclohexanamineoxide

Base Information

Chemical Name:(1S,2S,5R)-2-hydroxy-N,N,2-trimethyl-5-(prop-1-en-2-yl)cyclohexanamineoxide
CAS No.:1415961-21-5
Molecular Formula:C₁₂H₂₃NO₂
Molecular Weight:213.32
Hs Code.:

Synonyms:(1S,2S,5R)-2-hydroxy-N,N,2-trimethyl-5-(prop-1-en-2-yl)cyclohexanamineoxide

Suppliers and Price of (1S,2S,5R)-2-hydroxy-N,N,2-trimethyl-5-(prop-1-en-2-yl)cyclohexanamineoxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1S,2S,5R)-2-hydroxy-N,N,2-trimethyl-5-(prop-1-en-2-yl)cyclohexanamineoxide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (1S,2S,5R)-2-hydroxy-N,N,2-trimethyl-5-(prop-1-en-2-yl)cyclohexanamineoxide

There total 5 articles about (1S,2S,5R)-2-hydroxy-N,N,2-trimethyl-5-(prop-1-en-2-yl)cyclohexanamineoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 78478-85-0
(1S,2S,4R)-2-(dimethylamino)-1-methyl-4-(1-methylethenyl)cyclohexanol

: 1415961-21-5
(1S,2S,5R)-2-hydroxy-N,N,2-trimethyl-5-(prop-1-en-2-yl)cyclohexanamineoxide

Guidance literature:: With dihydrogen peroxide; In water; acetonitrile; at 20 ℃; for 2h; Cooling with ice;
DOI:10.1016/j.tetlet.2012.10.080

Reference yield:

: 5989-27-5,555-08-8,8022-90-0,9003-73-0,95327-98-3
D-limonene

: 1415961-21-5
(1S,2S,5R)-2-hydroxy-N,N,2-trimethyl-5-(prop-1-en-2-yl)cyclohexanamineoxide

Guidance literature:: Multi-step reaction with 3 steps

1: 3-chloro-benzenecarboperoxoic acid / chloroform / 1.5 h / -5 - 20 °C

2: water / 18 h / 20 °C / Reflux

3: dihydrogen peroxide / water; acetonitrile / 2 h / 20 °C / Cooling with ice

With dihydrogen peroxide; 3-chloro-benzenecarboperoxoic acid; In chloroform; water; acetonitrile;
DOI:10.1016/j.tetlet.2012.10.080

Reference yield:

: 1195-92-2
(4R)-limonene 1,2-epoxide

: 1415961-21-5
(1S,2S,5R)-2-hydroxy-N,N,2-trimethyl-5-(prop-1-en-2-yl)cyclohexanamineoxide

Guidance literature:: Multi-step reaction with 2 steps

1: water / 18 h / 20 °C / Reflux

2: dihydrogen peroxide / water; acetonitrile / 2 h / 20 °C / Cooling with ice

With dihydrogen peroxide; In water; acetonitrile;
DOI:10.1016/j.tetlet.2012.10.080