2-hydroxy-5-{(E)-[4-(propan-2-yl)phenyl]diazenyl}benzaldehyde

Base Information

• Chemical Name: 2-hydroxy-5-{(E)-[4-(propan-2-yl)phenyl]diazenyl}benzaldehyde
• CAS No.: 1606127-23-4
• Molecular Formula: C₁₆H₁₆N₂O₂
• Molecular Weight: 268.315
• Mol file: 1606127-23-4.mol

Synonyms:2-hydroxy-5-{(E)-[4-(propan-2-yl)phenyl]diazenyl}benzaldehyde

Chemical Property of 2-hydroxy-5-{(E)-[4-(propan-2-yl)phenyl]diazenyl}benzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-hydroxy-5-{(E)-[4-(propan-2-yl)phenyl]diazenyl}benzaldehyde

There total 1 articles about 2-hydroxy-5-{(E)-[4-(propan-2-yl)phenyl]diazenyl}benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

4-Isopropylaniline (99-88-7) + salicylaldehyde (90-02-8) → 2-hydroxy-5-{(E)-[4-(propan-2-yl)phenyl]diazenyl}benzaldehyde (1606127-23-4)

Guidance literature:

4-Isopropylaniline; With hydrogenchloride; sodium nitrite; In water; at -0.16 - 4.84 ℃; for 0.5h;

salicylaldehyde; In water; at -0.16 - 4.84 ℃; for 1h; pH=9 - 10;

DOI:10.1016/j.molstruc.2014.02.052

Reference yield: 73.0%

2-hydroxy-5-{(E)-[4-(propan-2-yl)phenyl]diazenyl}benzaldehyde (1606127-23-4) + nickel(II) acetate tetrahydrate (6018-89-9) → [Ni(ipr-salicylaldehyde)2] pentahydrate

Guidance literature:

In methanol; for 3h; Reflux;

DOI:10.1016/j.molstruc.2014.02.052

Reference yield: 70.84%

2-hydroxy-5-{(E)-[4-(propan-2-yl)phenyl]diazenyl}benzaldehyde (1606127-23-4) + 3,4-diaminofurazan (17220-38-1) → C34H32N8O3

Guidance literature:

2-hydroxy-5-{(E)-[4-(propan-2-yl)phenyl]diazenyl}benzaldehyde; 3,4-diaminofurazan; In methanol; at 60 - 70 ℃; for 1h;

With acetic acid; In methanol; water; at 60 - 70 ℃;

DOI:10.1016/j.saa.2014.04.181

upstream raw materials:

4-Isopropylaniline

salicylaldehyde