14-benzyl-7,8,13b,14-tetrahydroindolo[2',3':3,4]pyrido[2,1-b]quinazolin-5(13H)-one

Base Information

Chemical Name:14-benzyl-7,8,13b,14-tetrahydroindolo[2',3':3,4]pyrido[2,1-b]quinazolin-5(13H)-one
CAS No.:1316852-07-9
Molecular Formula:C₂₅H₂₁N₃O
Molecular Weight:379.461
Hs Code.:

Synonyms:14-benzyl-7,8,13b,14-tetrahydroindolo[2',3':3,4]pyrido[2,1-b]quinazolin-5(13H)-one

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Chemical Property of 14-benzyl-7,8,13b,14-tetrahydroindolo[2',3':3,4]pyrido[2,1-b]quinazolin-5(13H)-one

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Technology Process of 14-benzyl-7,8,13b,14-tetrahydroindolo[2',3':3,4]pyrido[2,1-b]quinazolin-5(13H)-one

There total 6 articles about 14-benzyl-7,8,13b,14-tetrahydroindolo[2',3':3,4]pyrido[2,1-b]quinazolin-5(13H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 4894-26-2
3,4-dihydro-β-carboline

: 35710-05-5
N-benzylisatoic anhydride

: 1316852-07-9
14-benzyl-7,8,13b,14-tetrahydroindolo[2',3':3,4]pyrido[2,1-b]quinazolin-5(13H)-one

Guidance literature:: In chloroform; for 8h; Reflux;
DOI:10.1016/j.tet.2011.05.120

Reference yield: 71.0%

: 1316852-07-9
14-benzyl-7,8,13b,14-tetrahydroindolo[2',3':3,4]pyrido[2,1-b]quinazolin-5(13H)-one

Guidance literature:: With boron trifluoride diethyl ether complex; In N,N-dimethyl-formamide; for 6h; Inert atmosphere;

Reference yield: 58.0%

: 61-54-1
tryptamine

: 35710-05-5
N-benzylisatoic anhydride

: 1316852-07-9
14-benzyl-7,8,13b,14-tetrahydroindolo[2',3':3,4]pyrido[2,1-b]quinazolin-5(13H)-one

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; trifluoroacetic anhydride; In N,N-dimethyl acetamide; at 100 ℃; for 5h;
DOI:10.1021/acs.orglett.8b02667