bis<2-(1-hydroxy-1-methylethyl)-4-(1,1-dimethylethyl)-6-(carbethoxy)phenyl> sulfoxide

Base Information

Chemical Name:bis<2-(1-hydroxy-1-methylethyl)-4-(1,1-dimethylethyl)-6-(carbethoxy)phenyl> sulfoxide
CAS No.:75894-01-8
Molecular Formula:C₃₂H₄₆O₇S
Molecular Weight:574.779
Hs Code.:

Synonyms:bis<2-(1-hydroxy-1-methylethyl)-4-(1,1-dimethylethyl)-6-(carbethoxy)phenyl> sulfoxide

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Chemical Property of bis<2-(1-hydroxy-1-methylethyl)-4-(1,1-dimethylethyl)-6-(carbethoxy)phenyl> sulfoxide

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Technology Process of bis<2-(1-hydroxy-1-methylethyl)-4-(1,1-dimethylethyl)-6-(carbethoxy)phenyl> sulfoxide

There total 6 articles about bis<2-(1-hydroxy-1-methylethyl)-4-(1,1-dimethylethyl)-6-(carbethoxy)phenyl> sulfoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 62558-12-7
bis<2-(1-hydroxy-1-methylethyl)-4-(1,1-dimethylethyl)-6-carbethoxyphenyl> sulphide

: 75894-01-8
bis<2-(1-hydroxy-1-methylethyl)-4-(1,1-dimethylethyl)-6-(carbethoxy)phenyl> sulfoxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 0.00833333h;
DOI:10.1021/ja00391a023

Reference yield:

: 64407-86-9
2-mercapto-5-tert-butylisophthalic acid

: 75894-01-8
bis<2-(1-hydroxy-1-methylethyl)-4-(1,1-dimethylethyl)-6-(carbethoxy)phenyl> sulfoxide

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / NaOH, copper-bronze powder / dimethylformamide / 14 h / Heating

2: SOCl₂ / Heating

3: pyridine / 1 h / Heating

4: 78.4 percent / diethyl ether / 3 h / Heating

5: 53 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 0.01 h

With pyridine; sodium hydroxide; thionyl chloride; copper; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00391a023

Reference yield:

: 62558-15-0
C₃₂H₄₂O₈S

: 75894-01-8
bis<2-(1-hydroxy-1-methylethyl)-4-(1,1-dimethylethyl)-6-(carbethoxy)phenyl> sulfoxide

Guidance literature:: Multi-step reaction with 2 steps

1: 78.4 percent / diethyl ether / 3 h / Heating

2: 53 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 0.01 h

With 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;
DOI:10.1021/ja00391a023