C₅₅H₄₇P₃PdSi

Base Information

Chemical Name:C₅₅H₄₇P₃PdSi
CAS No.:1198806-66-4
Molecular Formula:C₅₅H₄₇P₃PdSi
Molecular Weight:935.405
Hs Code.:

C<sub>55</sub>H<sub>47</sub>P<sub>3</sub>PdSi

Synonyms:C₅₅H₄₇P₃PdSi

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Chemical Property of C₅₅H₄₇P₃PdSi

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Technology Process of C₅₅H₄₇P₃PdSi

There total 9 articles about C₅₅H₄₇P₃PdSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1271-03-0
allyl(cyclopentadiene)palladium(II)

: 1002720-76-4
bis(o-(diphenylphosphino)phenyl)methylsilane

: 603-35-0
triphenylphosphine

: 1198806-66-4
[Pd(triphenylphosphine)(η2-Si-H-bis(o-(diphenylphosphino)phenyl)methylsilane)]

Guidance literature:: In tetrahydrofuran; diethyl ether; treatment of HSiMe(C6H4PPh2)2 with 1 equiv. of PPh3 and 1 equiv. of CpPd(C3H5) in Et2O-THF at room temp. for 20 min;
DOI:10.1021/om900874p

Reference yield: 86.0%

: 1271-03-0
allyl(cyclopentadiene)palladium(II)

: 1002720-76-4
bis(o-(diphenylphosphino)phenyl)methylsilane

: 603-35-0
triphenylphosphine

: 1198806-66-4
[Pd(η2-Si,H-bis(o-(diphenylphosphino)phenyl)methylsilane-κP,P')(triphenylphosphine)]

Guidance literature:: In tetrahydrofuran; diethyl ether; (Ar); addn. of palladium compd. to stirred soln. of silane deriv. and triphenylphosphine at room temp., stirring for 20 min; evapn. in vac., washing with ether, recrystn. (THF/pentane) at -30°C, elem. anal.;
DOI:10.1039/c1dt10526d

Reference yield: 70.0%

: 14221-01-3
tetrakis(triphenylphosphine) palladium⁽⁰⁾

: 1002720-76-4
bis(o-(diphenylphosphino)phenyl)methylsilane

: 1198806-66-4
[Pd(triphenylphosphine)(η2-Si-H-bis(o-(diphenylphosphino)phenyl)methylsilane)]

Guidance literature:: In tetrahydrofuran; mixing of HSiMe(C6H4PPh2)2 (1 equiv.) and Pd(PPh3)4 (1 equiv. ) in THF; stirring at room temp. for 30 min; removal of solvent under reduced pressure; washing with ether twice and recrystn. from THF-pentane at -30°C; elem. anal.;
DOI:10.1021/om900874p