3-(tert-butoxycarbonylamino)-1-(2-phenyl-1,3-dithian-2-yl)cyclohexyl acetate

Base Information

Chemical Name:3-(tert-butoxycarbonylamino)-1-(2-phenyl-1,3-dithian-2-yl)cyclohexyl acetate
CAS No.:1383796-96-0
Molecular Formula:C₂₃H₃₃NO₄S₂
Molecular Weight:451.651
Hs Code.:

Synonyms:3-(tert-butoxycarbonylamino)-1-(2-phenyl-1,3-dithian-2-yl)cyclohexyl acetate

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Chemical Property of 3-(tert-butoxycarbonylamino)-1-(2-phenyl-1,3-dithian-2-yl)cyclohexyl acetate

Chemical Property:

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Technology Process of 3-(tert-butoxycarbonylamino)-1-(2-phenyl-1,3-dithian-2-yl)cyclohexyl acetate

There total 1 articles about 3-(tert-butoxycarbonylamino)-1-(2-phenyl-1,3-dithian-2-yl)cyclohexyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 885280-38-6,1803033-61-5,1383797-87-2
(3-oxo-cyclohexyl)-carbamic acid tert-butyl ester

: 5425-44-5
2-Phenyl-[1,3]dithiane

: 108-24-7
acetic anhydride

: 1383796-96-0
3-(tert-butoxycarbonylamino)-1-(2-phenyl-1,3-dithian-2-yl)cyclohexyl acetate

Guidance literature:: 2-Phenyl-[1,3]dithiane; With lithium diisopropyl amide; In tetrahydrofuran; n-heptane; ethylbenzene; at -78 - -20 ℃; for 0.5h; Inert atmosphere;

(3-oxo-cyclohexyl)-carbamic acid tert-butyl ester; acetic anhydride; In tetrahydrofuran; n-heptane; ethylbenzene; at 20 ℃; for 4h;

With water; In tetrahydrofuran; n-heptane; ethylbenzene;

Reference yield:

: 1383796-96-0
3-(tert-butoxycarbonylamino)-1-(2-phenyl-1,3-dithian-2-yl)cyclohexyl acetate

: 1383797-02-1
(3-amino-1-hydroxycyclohexyl)(phenyl)methanone

Guidance literature:: 3-(tert-butoxycarbonylamino)-1-(2-phenyl-1,3-dithian-2-yl)cyclohexyl acetate; With nitrosonium tetrafluoroborate; pyridine hydrogenfluoride; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

With sodium carbonate;

Reference yield:

: 1383796-96-0
3-(tert-butoxycarbonylamino)-1-(2-phenyl-1,3-dithian-2-yl)cyclohexyl acetate

: 1383796-99-3
3-amino-1-(difluoro(phenyl)methyl)cyclohexanol

Guidance literature:: 3-(tert-butoxycarbonylamino)-1-(2-phenyl-1,3-dithian-2-yl)cyclohexyl acetate; With nitrosonium tetrafluoroborate; pyridine hydrogenfluoride; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

With sodium carbonate; In dichloromethane;