2-benzylsulfonylethyl-triphenylsilane

Base Information

• Chemical Name: 2-benzylsulfonylethyl-triphenylsilane
• CAS No.: 18870-60-5
• Molecular Formula: C₂₇H₂₆O₂SSi
• Molecular Weight: 442.654
• Mol file: 18870-60-5.mol

Synonyms:2-benzylsulfonylethyl-triphenylsilane

Chemical Property of 2-benzylsulfonylethyl-triphenylsilane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-benzylsulfonylethyl-triphenylsilane

There total 4 articles about 2-benzylsulfonylethyl-triphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2-benzylthioethyl-triphenylsilane (18870-33-2) → 2-benzylsulfonylethyl-triphenylsilane (18870-60-5)

Guidance literature:

With H₂O₂; In acetic acid; (C6H5)3SiCH2CH2SCH2C6H5 and H2O2 in glacial acetic acid at room temp. for several hours; reflux;; crystn. on cooling;;

DOI:10.1021/ja01111a045

Reference yield:

phenylmethanethiol (100-53-8) + vinyltriphenylsilane (18666-68-7) → 2-benzylsulfonylethyl-triphenylsilane (18870-60-5)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid

2: H₂O₂ / acetic acid

With H₂O₂; In acetic acid;

DOI:10.1021/ja01111a045

Reference yield:

phenylmethanethiol (100-53-8) → 2-benzylsulfonylethyl-triphenylsilane (18870-60-5)

Guidance literature:

Multi-step reaction with 2 steps

1: dibenzoyl peroxide

2: H₂O₂

With dihydrogen peroxide; dibenzoyl peroxide;

DOI:10.1021/ja01111a044

upstream raw materials:

2-benzylthioethyl-triphenylsilane

phenylmethanethiol

vinyltriphenylsilane