C₃₇H₄₀N₆O₅

Base Information

Chemical Name:C₃₇H₄₀N₆O₅
CAS No.:1312611-36-1
Molecular Formula:C₃₇H₄₀N₆O₅
Molecular Weight:648.762
Hs Code.:

C<sub>37</sub>H<sub>40</sub>N<sub>6</sub>O<sub>5</sub>

Synonyms:C₃₇H₄₀N₆O₅

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Chemical Property of C₃₇H₄₀N₆O₅

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Technology Process of C₃₇H₄₀N₆O₅

There total 11 articles about C₃₇H₄₀N₆O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 103-82-2
phenylacetic acid

: 1312611-35-0
C₂₉H₃₄N₆O₄

: 1312611-36-1
C₃₇H₄₀N₆O₅

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 5332-25-2
6-bromoquinoline

: 1312611-36-1
C₃₇H₄₀N₆O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 20 °C / Cooling with ice

2.1: chloro-trimethyl-silane; triethylamine / N,N-dimethyl-formamide / 100 °C

3.1: hydrogenchloride; water / 19 h / Reflux

4.1: triethylamine; diphenyl phosphoryl azide / N,N-dimethyl-formamide / 7 h / 100 °C

5.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C

6.1: HATU / N,N-dimethyl-formamide / 1 h / 20 °C

6.2: 20 °C

7.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 8 h / 100 - 110 °C

8.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; tetrahydrofuran / 80 °C

9.1: hydrogen / palladium 10% on activated carbon / methanol / 24 h / 20 °C / 1551.49 Torr

10.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With hydrogenchloride; chloro-trimethyl-silane; diphenyl phosphoryl azide; water; hydrogen; potassium acetate; sodium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; HATU; trifluoroacetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; 8.1: Suzuki Coupling;

Reference yield:

: 6563-11-7
6-bromoquinoline-N-oxide

: 1312611-36-1
C₃₇H₄₀N₆O₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: chloro-trimethyl-silane; triethylamine / N,N-dimethyl-formamide / 100 °C

2.1: hydrogenchloride; water / 19 h / Reflux

3.1: triethylamine; diphenyl phosphoryl azide / N,N-dimethyl-formamide / 7 h / 100 °C

4.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C

5.1: HATU / N,N-dimethyl-formamide / 1 h / 20 °C

5.2: 20 °C

6.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 8 h / 100 - 110 °C

7.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; tetrahydrofuran / 80 °C

8.1: hydrogen / palladium 10% on activated carbon / methanol / 24 h / 20 °C / 1551.49 Torr

9.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With hydrogenchloride; chloro-trimethyl-silane; diphenyl phosphoryl azide; water; hydrogen; potassium acetate; sodium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; 7.1: Suzuki Coupling;