18-O-allyl-2'-N-(4-nitrocinnamoyl)-Et 770

Base Information

• Chemical Name: 18-O-allyl-2'-N-(4-nitrocinnamoyl)-Et 770
• CAS No.: 1326247-91-9
• Molecular Formula: C₅₂H₅₁N₅O₁₃S
• Molecular Weight: 986.069
• Mol file: 1326247-91-9.mol

Synonyms:18-O-allyl-2'-N-(4-nitrocinnamoyl)-Et 770

Chemical Property of 18-O-allyl-2'-N-(4-nitrocinnamoyl)-Et 770

Chemical Property:

Purity/Quality:

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Technology Process of 18-O-allyl-2'-N-(4-nitrocinnamoyl)-Et 770

There total 1 articles about 18-O-allyl-2'-N-(4-nitrocinnamoyl)-Et 770 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.1%

18,6'-O-bisallyl-2'-N-(4''-nitrocinnamoyl)-ecteinascidin 770 (1326247-85-1) → 2'-N-(4''-nitrocinnamoyl)-ecteinascidin 770 (1326247-87-3) + 18-O-allyl-2'-N-(4-nitrocinnamoyl)-Et 770 (1326247-91-9)

Guidance literature:

18,6'-O-bisallyl-2'-N-(4''-nitrocinnamoyl)-ecteinascidin 770; With bis-triphenylphosphine-palladium(II) chloride; tri-n-butyl-tin hydride; acetic acid; In tetrahydrofuran; at 25 ℃; for 1h;

With sodium hydrogencarbonate; In tetrahydrofuran; water;

DOI:10.1016/j.bmc.2011.06.047

upstream raw materials:

18,6'-O-bisallyl-2'-N-(4''-nitrocinnamoyl)-ecteinascidin 770