tri-O-benzyl-α-L-fucopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl azide

Base Information

• Chemical Name: tri-O-benzyl-α-L-fucopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl azide
• CAS No.: 953780-99-9
• Molecular Formula: C₄₉H₅₀N₄O₁₁
• Molecular Weight: 870.956

Synonyms:tri-O-benzyl-α-L-fucopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl azide

Chemical Property of tri-O-benzyl-α-L-fucopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl azide

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Technology Process of tri-O-benzyl-α-L-fucopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl azide

There total 1 articles about tri-O-benzyl-α-L-fucopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2-acetamido-3,6-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl azide (162894-87-3) + 2,3,4-tri-O-benzyl-1-thio-β-L-fucopyranoside (167612-35-3) → tri-O-benzyl-α-L-fucopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl azide (953780-99-9)

Guidance literature:

With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In chloroform; at -15 ℃; for 1h;

DOI:10.1039/b708227d

Reference yield: 100.0%

tri-O-benzyl-α-L-fucopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl azide (953780-99-9) + α,ω-bis(O-propargyl)diethylene glycol (126422-57-9) → C108H114N8O25

Guidance literature:

copper(l) iodide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃;

DOI:10.1039/b708227d

Reference yield: 100.0%

tri-O-benzyl-α-L-fucopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl azide (953780-99-9) + α,ω-bis(O-propargyl)triethylene glycol (126422-58-0) → C110H118N8O26

Guidance literature:

copper(l) iodide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃;

DOI:10.1039/b708227d

upstream raw materials:

2-acetamido-3,6-di-O-benzoyl-2-deoxy-β-D-glucopyranosyl azide

2,3,4-tri-O-benzyl-1-thio-β-L-fucopyranoside

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