3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-3-C-methyl-α-D-ribo-hexofuranose

Base Information

Chemical Name:3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-3-C-methyl-α-D-ribo-hexofuranose
CAS No.:64638-70-6
Molecular Formula:C₁₇H₂₄O₄
Molecular Weight:292.375
Hs Code.:

Synonyms:3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-3-C-methyl-α-D-ribo-hexofuranose

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Chemical Property of 3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-3-C-methyl-α-D-ribo-hexofuranose

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Technology Process of 3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-3-C-methyl-α-D-ribo-hexofuranose

There total 7 articles about 3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-3-C-methyl-α-D-ribo-hexofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 98003-98-6
3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-3-C-methyl-α-D-ribo-hex-5-enofuranose

: 64638-70-6
3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-3-C-methyl-α-D-ribo-hexofuranose

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 2h; Ambient temperature;

Reference yield:

: 55533-86-3,120615-67-0
3-O-Benzyl-3-C-methyl-1,2-O-isopropylidene-α-D-allofuranose

: 64638-70-6
3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-3-C-methyl-α-D-ribo-hexofuranose

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 20 h / Ambient temperature

2: LiAlH₄ / diethyl ether / 1.) 5 h, reflux, 2.) 12 h, room temp.

3: 48 percent / PPh₃/imidazole/iodine / toluene / 3 h / Heating

4: 1.) butyllithium / 1.) THF/hexane, 1.5 h, -20 --> -30 deg C, 2.) 15 h, -50 deg C; 20 h, -20 deg C

With 1H-imidazole; lithium aluminium tetrahydride; n-butyllithium; iodine; triphenylphosphine; In pyridine; diethyl ether; toluene;

Reference yield:

: 98003-97-5
3-O-benzyl-1,2-O-isopropylidene-3-C-methyl-5,6-ditosyloxy-α-D-allofuranose

: 64638-70-6
3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-3-C-methyl-α-D-ribo-hexofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 73.9 percent / NaI / butan-2-one / 1.5 h / Heating

2: 100 percent / H₂ / 10 percent Pd-C / ethyl acetate / 2 h / Ambient temperature

With hydrogen; sodium iodide; palladium on activated charcoal; In ethyl acetate; butanone;