(1S,3R)-(-)-2-benzyl-3-methoxycarbonyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionamide

Base Information

Chemical Name:(1S,3R)-(-)-2-benzyl-3-methoxycarbonyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionamide
CAS No.:84094-77-9
Molecular Formula:C₂₃H₂₅N₃O₃
Molecular Weight:391.47
Hs Code.:

Synonyms:(1S,3R)-(-)-2-benzyl-3-methoxycarbonyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionamide

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Chemical Property of (1S,3R)-(-)-2-benzyl-3-methoxycarbonyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionamide

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Technology Process of (1S,3R)-(-)-2-benzyl-3-methoxycarbonyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionamide

There total 3 articles about (1S,3R)-(-)-2-benzyl-3-methoxycarbonyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.4%

: 84094-74-6
(1S,3R)-(-)-methyl 2-benzyl-3-methoxycarbonyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionate

: 84094-76-8
(1S,3R)-(-)-2-benzyl-3-(amide)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionamide

: 84094-77-9
(1S,3R)-(-)-2-benzyl-3-methoxycarbonyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionamide

Guidance literature:: With ammonia; In methanol; for 480h; Ambient temperature;

Reference yield:

: 84094-72-4
(1S,3R)-(-)-2-benzyl-3-methoxycarbonyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionic acid

: 84094-77-9
(1S,3R)-(-)-2-benzyl-3-methoxycarbonyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂; methanol; diethyl ether

2: 11.9 percent / NH₃ / methanol / 480 h / Ambient temperature

With ammonia; In methanol; diethyl ether; dichloromethane;

Reference yield:

: 60702-97-8,84094-72-4,84094-73-5,91926-17-9
(-)-2-benzyl-3-methoxycarbonyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionic acid

: 84094-77-9
(1S,3R)-(-)-2-benzyl-3-methoxycarbonyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: 78.6 percent / diethyl ether; CH₂Cl₂; methanol / 1 h

2: 11.9 percent / ammonia gas / methanol / 480 h / Ambient temperature

With ammonia; In methanol; diethyl ether; dichloromethane;
DOI:10.1248/cpb.32.1313