2-(4-(5-oxo-5-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)pentyl)piperazin-1-yl)acetic acid

Base Information

• Chemical Name: 2-(4-(5-oxo-5-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)pentyl)piperazin-1-yl)acetic acid
• CAS No.: 1620517-37-4
• Molecular Formula: C₃₀H₃₉N₅O₄
• Molecular Weight: 533.671

Synonyms:2-(4-(5-oxo-5-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)pentyl)piperazin-1-yl)acetic acid

Chemical Property of 2-(4-(5-oxo-5-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)pentyl)piperazin-1-yl)acetic acid

Chemical Property:

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Technology Process of 2-(4-(5-oxo-5-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)pentyl)piperazin-1-yl)acetic acid

There total 2 articles about 2-(4-(5-oxo-5-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)pentyl)piperazin-1-yl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C20H20IN3O2 (1620517-34-1) + piperazine-1-acetic acid tert-butyl ester (112257-22-4) → 2-(4-(5-oxo-5-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)pentyl)piperazin-1-yl)acetic acid (1620517-37-4)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; acetonitrile; at 20 ℃; for 36h;

DOI:10.1016/j.ejmech.2014.06.011

Reference yield:

bromoacetic acid tert-butyl ester (5292-43-3) → 2-(4-(5-oxo-5-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)pentyl)piperazin-1-yl)acetic acid (1620517-37-4)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 20 h / 20 °C

2: potassium carbonate / acetonitrile; tetrahydrofuran / 36 h / 20 °C

With potassium carbonate; In tetrahydrofuran; ethanol; acetonitrile;

DOI:10.1016/j.ejmech.2014.06.011

Reference yield:

2-(4-(5-oxo-5-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)pentyl)piperazin-1-yl)acetic acid (1620517-37-4) → 2-(4-(5-oxo-5-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)pentyl)piperazin-1-yl)acetic acid (1620517-04-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 4h;

DOI:10.1016/j.ejmech.2014.06.011

upstream raw materials:

bromoacetic acid tert-butyl ester

C₂₀H₂₀IN₃O₂

piperazine-1-acetic acid tert-butyl ester

Downstream raw materials:

2-(4-(5-oxo-5-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)pentyl)piperazin-1-yl)acetic acid

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