N-[(3,3-dimethylcycloprop-1-enyl)phenylmethyl]-4-methylbenzenesulfonamide

Base Information

• Chemical Name: N-[(3,3-dimethylcycloprop-1-enyl)phenylmethyl]-4-methylbenzenesulfonamide
• CAS No.: 1245616-70-9
• Molecular Formula: C₁₉H₂₁NO₂S
• Molecular Weight: 327.447

Synonyms:N-[(3,3-dimethylcycloprop-1-enyl)phenylmethyl]-4-methylbenzenesulfonamide

Chemical Property of N-[(3,3-dimethylcycloprop-1-enyl)phenylmethyl]-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of N-[(3,3-dimethylcycloprop-1-enyl)phenylmethyl]-4-methylbenzenesulfonamide

There total 1 articles about N-[(3,3-dimethylcycloprop-1-enyl)phenylmethyl]-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

N-(benzylidene)-p-methylbenzenesulfonamide (51608-60-7) + 1,1,3‐tribromo‐2,2‐dimethylcyclopropane (23534-97-6) → N-[(3,3-dimethylcycloprop-1-enyl)phenylmethyl]-4-methylbenzenesulfonamide (1245616-70-9)

Guidance literature:

1,1,3‐tribromo‐2,2‐dimethylcyclopropane; With n-butyllithium; In diethyl ether; hexane; at -78 - -10 ℃;

N-(benzylidene)-p-methylbenzenesulfonamide; In diethyl ether; hexane; at -50 - 20 ℃;

With water; In diethyl ether; hexane; at 20 ℃;

DOI:10.1021/ol101741f

Reference yield: 100.0%

2-methyl-3-bromo-1-propene (1458-98-6) + N-[(3,3-dimethylcycloprop-1-enyl)phenylmethyl]-4-methylbenzenesulfonamide (1245616-70-9) → N-[(3,3-dimethylcycloprop-1-enyl)phenylmethyl]-4-methyl-N-(2-methylallyl)benzenesulfonamide (1245616-53-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

DOI:10.1021/ol101741f

Reference yield: 100.0%

N-[(3,3-dimethylcycloprop-1-enyl)phenylmethyl]-4-methylbenzenesulfonamide (1245616-70-9) + allyl bromide (106-95-6) → N-allyl-N-[(3,3-dimethylcycloprop-1-enyl)phenylmethyl]-4-methylbenzenesulfonamide (1245616-52-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 2.5h;

DOI:10.1021/ol101741f

upstream raw materials:

N-(benzylidene)-p-methylbenzenesulfonamide

1,1,3‐tribromo‐2,2‐dimethylcyclopropane

Downstream raw materials:

N-[(3,3-dimethylcycloprop-1-enyl)phenylmethyl]-4-methyl-N-(2-methylallyl)benzenesulfonamide

N-allyl-N-[(3,3-dimethylcycloprop-1-enyl)phenylmethyl]-4-methylbenzenesulfonamide

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