2-[(7-methoxy-tetradec-4-enoyl)-methyl-amino]-propionic acid benzyl ester

Base Information

Chemical Name:2-[(7-methoxy-tetradec-4-enoyl)-methyl-amino]-propionic acid benzyl ester
CAS No.:936445-88-4
Molecular Formula:C₂₆H₄₁NO₄
Molecular Weight:431.616
Hs Code.:

Synonyms:2-[(7-methoxy-tetradec-4-enoyl)-methyl-amino]-propionic acid benzyl ester

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Chemical Property of 2-[(7-methoxy-tetradec-4-enoyl)-methyl-amino]-propionic acid benzyl ester

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Technology Process of 2-[(7-methoxy-tetradec-4-enoyl)-methyl-amino]-propionic acid benzyl ester

There total 8 articles about 2-[(7-methoxy-tetradec-4-enoyl)-methyl-amino]-propionic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 936445-79-3
(R)-Lyngbic acid

: methylalanine benzyl ester hydrochloride

: 936445-88-4
2-[(7-methoxy-tetradec-4-enoyl)-methyl-amino]-propionic acid benzyl ester

Guidance literature:: With 2-chloro-1,3-dimethyl-2-imidazolium PF₆; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 14h;
DOI:10.1016/j.tet.2007.01.035

Reference yield:

: 936445-78-2
(R,E)-7-methoxytetradec-4-en-1-ol

: 936445-88-4
2-[(7-methoxy-tetradec-4-enoyl)-methyl-amino]-propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / CrO₃; H₂SO₄ / acetone / 0.5 h / 0 °C

2: 96 percent / 2-chloro-1,3-dimethyl-2-imidazolium PF₆; i-Pr₂NEt / CH₂Cl₂ / 14 h / 0 - 20 °C

With chromium(VI) oxide; 2-chloro-1,3-dimethyl-2-imidazolium PF₆; sulfuric acid; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetone;
DOI:10.1016/j.tet.2007.01.035

Reference yield:

: 934197-87-2
(R,E)-2-(7-methoxytetradec-4-enyloxy)-tetrahydro-2H-pyran

: 936445-88-4
2-[(7-methoxy-tetradec-4-enoyl)-methyl-amino]-propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / p-toluene sulfonic acid monohydrate / methanol / 3 h / 40 °C

2: 93 percent / CrO₃; H₂SO₄ / acetone / 0.5 h / 0 °C

3: 96 percent / 2-chloro-1,3-dimethyl-2-imidazolium PF₆; i-Pr₂NEt / CH₂Cl₂ / 14 h / 0 - 20 °C

With chromium(VI) oxide; 2-chloro-1,3-dimethyl-2-imidazolium PF₆; sulfuric acid; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; acetone;
DOI:10.1016/j.tet.2007.01.035