3-methyl-5-{3-[4-(methylsulfanyl)phenyl]-1-benzofuran-5-yl}-1,2,4-oxadiazole

Base Information

• Chemical Name: 3-methyl-5-{3-[4-(methylsulfanyl)phenyl]-1-benzofuran-5-yl}-1,2,4-oxadiazole
• CAS No.: 1191885-59-2
• Molecular Formula: C₁₈H₁₄N₂O₂S
• Molecular Weight: 322.387

Synonyms:3-methyl-5-{3-[4-(methylsulfanyl)phenyl]-1-benzofuran-5-yl}-1,2,4-oxadiazole

Chemical Property of 3-methyl-5-{3-[4-(methylsulfanyl)phenyl]-1-benzofuran-5-yl}-1,2,4-oxadiazole

Chemical Property:

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Technology Process of 3-methyl-5-{3-[4-(methylsulfanyl)phenyl]-1-benzofuran-5-yl}-1,2,4-oxadiazole

There total 1 articles about 3-methyl-5-{3-[4-(methylsulfanyl)phenyl]-1-benzofuran-5-yl}-1,2,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

methyl 3-[4-(methylsulfanyl)phenyl]-1-benzofuran-5-carboxylate (1005206-23-4) + acetamide oxime (118493-85-9,117771-39-8,1141922-26-0,1429624-21-4) → 3-methyl-5-{3-[4-(methylsulfanyl)phenyl]-1-benzofuran-5-yl}-1,2,4-oxadiazole (1191885-59-2)

Guidance literature:

acetamide oxime; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 - 60 ℃; for 0.75h;

methyl 3-[4-(methylsulfanyl)phenyl]-1-benzofuran-5-carboxylate; In tetrahydrofuran; mineral oil; at 60 ℃; for 2h;

DOI:10.1021/jm900647e

Reference yield: 91.0%

3-methyl-5-{3-[4-(methylsulfanyl)phenyl]-1-benzofuran-5-yl}-1,2,4-oxadiazole (1191885-59-2) → 3-methyl-5-{3-[4-(methylsulfinyl)phenyl]-1-benzofuran-5-yl}-1,2,4-oxadiazole (1191885-60-5)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 0.0833333h;

DOI:10.1021/jm900647e

upstream raw materials:

methyl 3-[4-(methylsulfanyl)phenyl]-1-benzofuran-5-carboxylate

acetamide oxime

Downstream raw materials:

3-methyl-5-{3-[4-(methylsulfinyl)phenyl]-1-benzofuran-5-yl}-1,2,4-oxadiazole

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