O-benzyl furanodictine A

Base Information

Chemical Name:O-benzyl furanodictine A
CAS No.:677334-87-1
Molecular Formula:C₂₀H₂₇NO₆
Molecular Weight:377.437
Hs Code.:

Synonyms:O-benzyl furanodictine A

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Chemical Property of O-benzyl furanodictine A

Chemical Property:

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Technology Process of O-benzyl furanodictine A

There total 11 articles about O-benzyl furanodictine A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 503-74-2
3-methylbutyric acid

: 677334-88-2
N-((3R,3aR,6R,6aR)-2-Benzyloxy-6-hydroxy-hexahydro-furo[3,2-b]furan-3-yl)-acetamide

: 677334-87-1
O-benzyl furanodictine A

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1016/j.tetlet.2003.12.135

Reference yield:

: 157831-25-9
(2R,3R,4R,5S)-1,3,4-Tris-benzyloxy-5-(4-methoxy-benzylamino)-hept-6-en-2-ol

: 677334-87-1
O-benzyl furanodictine A

Guidance literature:: Multi-step reaction with 13 steps

1.1: CH₂Cl₂

1.2: 50 percent / K₂CO₃ / methanol

2.1: 49 percent / CAN / methanol

3.1: 99 percent / OsO₄; NMO / acetone; H₂O

4.1: 90 percent / p-TsOH / acetone

5.1: 94 percent / (i-Pr)2NEt / CH₂Cl₂

6.1: 97 percent / H₂ / Pd/C / methanol

7.1: 79 percent / Bu₂SnO; Et₃N / CH₂Cl₂

8.1: 96 percent / K₂CO₃ / methanol

9.1: 82 percent / cc. HCl / methanol

10.1: 92 percent / NaIO₄ / diethyl ether; H₂O

11.1: 77 percent / Ag₂O / ethyl acetate

12.1: 78 percent / cc. HCl / methanol

13.1: 94 percent / EDCI; DMAP / CH₂Cl₂

With hydrogenchloride; dmap; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; ammonium cerium(IV) nitrate; hydrogen; di(n-butyl)tin oxide; potassium carbonate; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; silver(l) oxide; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane; water; ethyl acetate; acetone;
DOI:10.1016/j.tetlet.2003.12.135

Reference yield:

: 677334-92-8
N-[(1S,2R,3R,4R)-2,3,5-Tris-benzyloxy-1-(1,2-dihydroxy-ethyl)-4-hydroxy-pentyl]-acetamide

: 677334-87-1
O-benzyl furanodictine A

Guidance literature:: Multi-step reaction with 10 steps

1: 90 percent / p-TsOH / acetone

2: 94 percent / (i-Pr)2NEt / CH₂Cl₂

3: 97 percent / H₂ / Pd/C / methanol

4: 79 percent / Bu₂SnO; Et₃N / CH₂Cl₂

5: 96 percent / K₂CO₃ / methanol

6: 82 percent / cc. HCl / methanol

7: 92 percent / NaIO₄ / diethyl ether; H₂O

8: 77 percent / Ag₂O / ethyl acetate

9: 78 percent / cc. HCl / methanol

10: 94 percent / EDCI; DMAP / CH₂Cl₂

With hydrogenchloride; dmap; sodium periodate; hydrogen; di(n-butyl)tin oxide; potassium carbonate; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; silver(l) oxide; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane; water; ethyl acetate; acetone;
DOI:10.1016/j.tetlet.2003.12.135