[1-(2,4-dimethoxy-benzylthiocarbamoyl)-2-(1H-indol-3-yl)-ethyl]-carbamic acid tert-butyl ester

Base Information

• Chemical Name: [1-(2,4-dimethoxy-benzylthiocarbamoyl)-2-(1H-indol-3-yl)-ethyl]-carbamic acid tert-butyl ester
• CAS No.: 1007846-21-0
• Molecular Formula: C₂₅H₃₁N₃O₄S
• Molecular Weight: 469.605

Synonyms:[1-(2,4-dimethoxy-benzylthiocarbamoyl)-2-(1H-indol-3-yl)-ethyl]-carbamic acid tert-butyl ester

Chemical Property of [1-(2,4-dimethoxy-benzylthiocarbamoyl)-2-(1H-indol-3-yl)-ethyl]-carbamic acid tert-butyl ester

Chemical Property:

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Technology Process of [1-(2,4-dimethoxy-benzylthiocarbamoyl)-2-(1H-indol-3-yl)-ethyl]-carbamic acid tert-butyl ester

There total 1 articles about [1-(2,4-dimethoxy-benzylthiocarbamoyl)-2-(1H-indol-3-yl)-ethyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C25H31N3O5 (1007846-09-4) → [1-(2,4-dimethoxy-benzylthiocarbamoyl)-2-(1H-indol-3-yl)-ethyl]-carbamic acid tert-butyl ester (1007846-21-0)

Guidance literature:

With Lawessons reagent; In 1,2-dimethoxyethane; at 85 ℃;

DOI:10.1016/j.bmcl.2007.10.113

Reference yield: 55.0%

1H-indol-3-acetohydrazide (5448-47-5) + [1-(2,4-dimethoxy-benzylthiocarbamoyl)-2-(1H-indol-3-yl)-ethyl]-carbamic acid tert-butyl ester (1007846-21-0) → [1-[4-(2,4-dimethoxy-benzyl)-5-(1H-indol-3-ylmethyl)-4H-[1,2,4]triazol-3-yl]-2-(1H-indol-3-yl)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:

With mercury(II) diacetate; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/ol035778e

Reference yield:

3-phenylpropanehydrazide (3538-68-9) + [1-(2,4-dimethoxy-benzylthiocarbamoyl)-2-(1H-indol-3-yl)-ethyl]-carbamic acid tert-butyl ester (1007846-21-0) → C34H39N5O4 (1007846-45-8)

Guidance literature:

With mercury(II) diacetate; In tetrahydrofuran; at 20 ℃; for 48h;

DOI:10.1016/j.bmcl.2007.10.113

upstream raw materials:

C₂₅H₃₁N₃O₅

Downstream raw materials:

C₃₆H₄₀N₆O₄

C₃₄H₃₉N₅O₄

C₃₃H₃₇N₅O₄

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