Technology Process of C32H40O5
There total 5 articles about C32H40O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
zinc;
In
diethyl ether; N,N-dimethyl-formamide;
for 5h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trimethyl orthoformate / toluene-4-sulfonic acid / methanol / 20 °C
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C
2.2: -78 - 20 °C
3.1: zinc / diethyl ether; N,N-dimethyl-formamide / 5 h
With
oxalyl dichloride; dimethyl sulfoxide; zinc; trimethyl orthoformate;
toluene-4-sulfonic acid;
In
methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C
2.1: trimethyl orthoformate / toluene-4-sulfonic acid / methanol / 20 °C
3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C
3.2: -78 - 20 °C
4.1: zinc / diethyl ether; N,N-dimethyl-formamide / 5 h
With
oxalyl dichloride; potassium carbonate; dimethyl sulfoxide; zinc; trimethyl orthoformate;
toluene-4-sulfonic acid;
In
methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;