¹³C-N-mesitylimidazole

Base Information

• Chemical Name: ¹³C-N-mesitylimidazole
• CAS No.: 1101127-71-2
• Molecular Formula: C₁₂H₁₄N₂
• Molecular Weight: 187.246
• Mol file: 1101127-71-2.mol

Synonyms:¹³C-N-mesitylimidazole

Chemical Property of ¹³C-N-mesitylimidazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ¹³C-N-mesitylimidazole

There total 1 articles about ¹³C-N-mesitylimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

Glyoxal (131543-46-9,107-22-2) + [13C]-formaldehyde (3228-27-1,89277-65-6) + 2,4,6-trimethylaniline (88-05-1) → 13C-N-mesitylimidazole (1101127-71-2)

Guidance literature:

With ammonium acetate; In water; acetic acid; at 70 ℃; for 19.3h; Inert atmosphere;

DOI:10.1021/om300340w

Reference yield: 95.0%

1,3-propanesultone (1120-71-4) + 13C-N-mesitylimidazole (1101127-71-2) → 1-mesityl-3-(3-sulfonatopropyl)-2-13C-imidazolium

Guidance literature:

In acetone; at 20 ℃; for 120h; Inert atmosphere; Schlenk technique;

DOI:10.1002/anie.201407758

Reference yield: 68.0%

methyl bromide (74-83-9) + 13C-N-mesitylimidazole (1101127-71-2) → (13)C-N-mesityl-N'-methylimidazolium chloride (1375015-46-5)

Guidance literature:

In tert-butyl methyl ether; acetonitrile; at 60 ℃; for 20h;

DOI:10.1021/om300340w

upstream raw materials:

Glyoxal

[13C]-formaldehyde

2,4,6-trimethylaniline

Downstream raw materials:

⁽¹³⁾C-N-mesityl-N'-methylimidazolium chloride

⁽¹³⁾C-N-mesityl-N'-methylimidazolium chloride