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C36H40N4O7S2

Base Information
  • Chemical Name:C36H40N4O7S2
  • CAS No.:1094172-72-1
  • Molecular Formula:C36H40N4O7S2
  • Molecular Weight:704.868
  • Hs Code.:
C<sub>36</sub>H<sub>40</sub>N<sub>4</sub>O<sub>7</sub>S<sub>2</sub>

Synonyms:C36H40N4O7S2

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Chemical Property of C36H40N4O7S2
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Technology Process of C36H40N4O7S2

There total 16 articles about C36H40N4O7S2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With lithium borohydride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1002/ejoc.201100242
Guidance literature:
Multi-step reaction with 10 steps
1: acetic acid; zinc / water / 1.83 h / 80 - 85 °C
2: glyoxylic acid ethyl ester; magnesium sulfate / dichloromethane / 0 - 20 °C
3: dmap; triethylamine / toluene / 18 h / 70 °C
4: ammonium cerium (IV) nitrate / water; acetonitrile / 0.25 h / -15 °C
5: dichloromethane / 4 h / 20 °C
6: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / 1,4-dioxane / 21 h / 100 °C
7: tetrabutyl ammonium fluoride / tetrahydrofuran; water / 0.33 h / 0 °C
8: hydrogen bromide; acetic acid / tetrahydrofuran / 0.5 h / 0 °C
9: tetrakis(triphenylphosphine) palladium(0); sodium ethanolate; caesium carbonate / 1,4-dioxane / 4 h / 100 °C
10: lithium borohydride / tetrahydrofuran / 0 - 20 °C
With dmap; copper(l) iodide; lithium borohydride; tetrakis(triphenylphosphine) palladium(0); glyoxylic acid ethyl ester; ammonium cerium (IV) nitrate; tetrabutyl ammonium fluoride; hydrogen bromide; sodium ethanolate; magnesium sulfate; caesium carbonate; acetic acid; triethylamine; zinc; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene; acetonitrile; 6: Sonogashira coupling / 9: Suzuki-Miyaura cross-coupling reaction;
DOI:10.1002/ejoc.201100242
Guidance literature:
Multi-step reaction with 5 steps
1: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / 1,4-dioxane / 21 h / 100 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran; water / 0.33 h / 0 °C
3: hydrogen bromide; acetic acid / tetrahydrofuran / 0.5 h / 0 °C
4: tetrakis(triphenylphosphine) palladium(0); sodium ethanolate; caesium carbonate / 1,4-dioxane / 4 h / 100 °C
5: lithium borohydride / tetrahydrofuran / 0 - 20 °C
With copper(l) iodide; lithium borohydride; tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride; hydrogen bromide; sodium ethanolate; caesium carbonate; acetic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; water; 1: Sonogashira coupling / 4: Suzuki-Miyaura cross-coupling reaction;
DOI:10.1002/ejoc.201100242
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