1-(4-Methylphenyl)sulfonylbenzo[cd]indol-2-one

Base Information

Chemical Name:1-(4-Methylphenyl)sulfonylbenzo[cd]indol-2-one
CAS No.:119200-14-5
Molecular Formula:C₁₈H₁₃NO₃S
Molecular Weight:323.372
Hs Code.:
DSSTox Substance ID:DTXSID001322388
ChEMBL ID:CHEMBL1350814

Synonyms:MLS000773549;CHEMBL1350814;DTXSID001322388;HMS2744A10;AKOS003624045;SMR000364250;1-(4-methylphenyl)sulfonylbenzo[cd]indol-2-one;Z56784408;119200-14-5

Suppliers and Price of 1-(4-Methylphenyl)sulfonylbenzo[cd]indol-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-Methylphenyl)sulfonylbenzo[cd]indol-2-one

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:323.06161445
Heavy Atom Count:23
Complexity:574

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)N2C3=CC=CC4=C3C(=CC=C4)C2=O

Technology Process of 1-(4-Methylphenyl)sulfonylbenzo[cd]indol-2-one

There total 6 articles about 1-(4-Methylphenyl)sulfonylbenzo[cd]indol-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: C₂₂H₂₃NO₂SSi

: 119200-14-5
1-(toluene-4-sulfonyl)-1H-benz[cd]indol-2-one

Guidance literature:: With tert.-butylhydroperoxide; copper(l) iodide; In dimethyl sulfoxide; at 110 ℃;
DOI:10.1021/acs.joc.0c01725

Reference yield: 54.0%

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 18271-17-5
N-tosyl-1-naphthylamine

: 119200-14-5
1-(toluene-4-sulfonyl)-1H-benz[cd]indol-2-one

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; oxygen; copper diacetate; In N,N-dimethyl-formamide; at 100 ℃; for 16h; under 760.051 Torr; Inert atmosphere;
DOI:10.1021/ol2023856

Reference yield:

: 134-32-7
1-amino-naphthalene

: 119200-14-5
1-(toluene-4-sulfonyl)-1H-benz[cd]indol-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 12 h / Reflux

2: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; oxygen; copper diacetate / N,N-dimethyl-formamide / 16 h / 100 °C / 760.05 Torr / Inert atmosphere

With pyridine; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; oxygen; copper diacetate; In N,N-dimethyl-formamide;
DOI:10.1021/ol2023856