Technology Process of C49H36P2
There total 4 articles about C49H36P2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen bromide; sodium nitrite / water / 0 °C
2.1: hydrogen bromide; copper(I) bromide / water / 0 - 100 °C
3.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere
3.2: -78 - 20 °C / Inert atmosphere
With
n-butyllithium; hydrogen bromide; copper(I) bromide; sodium nitrite;
In
tetrahydrofuran; water;
DOI:10.1002/chem.201003434
- Guidance literature:
-
9,9-bis(4-bromophenyl)-9H-fluorene;
With
n-butyllithium;
In
tetrahydrofuran;
at -78 ℃;
Inert atmosphere;
chloro-diphenylphosphine;
In
tetrahydrofuran;
at -78 - 20 ℃;
Inert atmosphere;
DOI:10.1002/chem.201003434
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride; water / 24 h / 140 °C
2.1: hydrogen bromide; sodium nitrite / water / 0 °C
3.1: hydrogen bromide; copper(I) bromide / water / 0 - 100 °C
4.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere
4.2: -78 - 20 °C / Inert atmosphere
With
hydrogenchloride; n-butyllithium; water; hydrogen bromide; copper(I) bromide; sodium nitrite;
In
tetrahydrofuran; water;
DOI:10.1002/chem.201003434