methyl 3-[(tert-butoxycarbonyl)(cyclopropylmethyl)amino]-5-hydroxybenzoate

Base Information

Chemical Name:methyl 3-[(tert-butoxycarbonyl)(cyclopropylmethyl)amino]-5-hydroxybenzoate
CAS No.:1310807-51-2
Molecular Formula:C₁₇H₂₃NO₅
Molecular Weight:321.373
Hs Code.:

Synonyms:methyl 3-[(tert-butoxycarbonyl)(cyclopropylmethyl)amino]-5-hydroxybenzoate

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Chemical Property of methyl 3-[(tert-butoxycarbonyl)(cyclopropylmethyl)amino]-5-hydroxybenzoate

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Technology Process of methyl 3-[(tert-butoxycarbonyl)(cyclopropylmethyl)amino]-5-hydroxybenzoate

There total 3 articles about methyl 3-[(tert-butoxycarbonyl)(cyclopropylmethyl)amino]-5-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1310807-50-1
methyl 3-(benzyloxy)-5-[(tert-butoxycarbonyl)(cyclopropylmethyl)amino]benzoate

: 1310807-51-2
methyl 3-[(tert-butoxycarbonyl)(cyclopropylmethyl)amino]-5-hydroxybenzoate

Guidance literature:: With cyclohexene; 20% palladium hydroxide-activated charcoal; In tetrahydrofuran; ethanol; for 1.5h; Reflux;

Reference yield:

: methyl 3-(benzyloxy)-5-[(tert-butoxycarbonyl)amino]benzoate

: 1310807-51-2
methyl 3-[(tert-butoxycarbonyl)(cyclopropylmethyl)amino]-5-hydroxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / N,N-dimethyl-formamide / 3.33 h / 15 - 20 °C / Cooling with ice

2: cyclohexene / 20% palladium hydroxide-activated charcoal / ethanol; tetrahydrofuran / 1.5 h / Reflux

With potassium tert-butylate; cyclohexene; 20% palladium hydroxide-activated charcoal; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 53478-05-0
3-(benzyloxy)-5-(methoxycarbonyl)benzoic acid

: 1310807-51-2
methyl 3-[(tert-butoxycarbonyl)(cyclopropylmethyl)amino]-5-hydroxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; diphenyl phosphoryl azide / 2 h / 105 °C

2: potassium tert-butylate / N,N-dimethyl-formamide / 3.33 h / 15 - 20 °C / Cooling with ice

3: cyclohexene / 20% palladium hydroxide-activated charcoal / ethanol; tetrahydrofuran / 1.5 h / Reflux

With diphenyl phosphoryl azide; potassium tert-butylate; triethylamine; cyclohexene; 20% palladium hydroxide-activated charcoal; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;