N-(2,2-dimethyl-5-phenyl[1,3]dioxan-5-yl)-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine

Base Information

Chemical Name:N-(2,2-dimethyl-5-phenyl[1,3]dioxan-5-yl)-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine
CAS No.:861198-46-1
Molecular Formula:C₃₀H₃₇NO₃
Molecular Weight:459.629
Hs Code.:

Synonyms:N-(2,2-dimethyl-5-phenyl[1,3]dioxan-5-yl)-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine

Suppliers and Price of N-(2,2-dimethyl-5-phenyl[1,3]dioxan-5-yl)-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(2,2-dimethyl-5-phenyl[1,3]dioxan-5-yl)-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(2,2-dimethyl-5-phenyl[1,3]dioxan-5-yl)-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine

There total 6 articles about N-(2,2-dimethyl-5-phenyl[1,3]dioxan-5-yl)-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 861198-45-0
2,2-dimethyl-5-nitroxide-N-(2-methyl-1-phenylpropyl)-5-phenyl[1,3]dioxane

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 861198-46-1
N-(2,2-dimethyl-5-phenyl[1,3]dioxan-5-yl)-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine

Guidance literature:: With sodium tetrahydroborate; Jacobsen's catalyst; In ethanol; toluene; at 20 ℃;
DOI:10.1055/s-2005-869894

Reference yield:

: 5428-02-4
2-nitro-2-phenyl-propane-1,3-diol

: 861198-46-1
N-(2,2-dimethyl-5-phenyl[1,3]dioxan-5-yl)-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / p-TsOH*H₂O; 4 Angstroem molecular sieves / tetrahydrofuran / 12 h / Heating

2: 67 percent / Zn; aq. NH₄Cl / diethyl ether / 20 °C

3: tetrahydrofuran / 2 h / 20 °C

4: 610 mg / Cu(OAc)2*H₂O; NH₄Cl; air / methanol

5: 44 percent / NaBH₄ / Jacobsen's catalyst / toluene; ethanol / 20 °C

With sodium tetrahydroborate; copper diacetate; air; 4 A molecular sieve; ammonium chloride; toluene-4-sulfonic acid; zinc; Jacobsen's catalyst; In tetrahydrofuran; methanol; diethyl ether; ethanol; toluene; 3: Grignard addition;
DOI:10.1055/s-2005-869894

Reference yield:

: 37561-37-8
2,2-dimethyl-5-nitro-5-phenyl[1,3]dioxane

: 861198-46-1
N-(2,2-dimethyl-5-phenyl[1,3]dioxan-5-yl)-N-(2-methyl-1-phenylpropyl)-O-(1-phenylethyl)hydroxylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / Zn; aq. NH₄Cl / diethyl ether / 20 °C

2: tetrahydrofuran / 2 h / 20 °C

3: 610 mg / Cu(OAc)2*H₂O; NH₄Cl; air / methanol

4: 44 percent / NaBH₄ / Jacobsen's catalyst / toluene; ethanol / 20 °C

With sodium tetrahydroborate; copper diacetate; air; ammonium chloride; zinc; Jacobsen's catalyst; In tetrahydrofuran; methanol; diethyl ether; ethanol; toluene; 2: Grignard addition;
DOI:10.1055/s-2005-869894