{(2R,3R)-3-[(S)-2-(4-Methoxy-benzyloxy)-1-methyl-ethyl]-2-methyl-oxiranyl}-methanol

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Chemical Name:{(2R,3R)-3-[(S)-2-(4-Methoxy-benzyloxy)-1-methyl-ethyl]-2-methyl-oxiranyl}-methanol
CAS No.:220213-63-8
Molecular Formula:C₁₅H₂₂O₄
Molecular Weight:266.337
Hs Code.:

Synonyms:{(2R,3R)-3-[(S)-2-(4-Methoxy-benzyloxy)-1-methyl-ethyl]-2-methyl-oxiranyl}-methanol

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Chemical Property of {(2R,3R)-3-[(S)-2-(4-Methoxy-benzyloxy)-1-methyl-ethyl]-2-methyl-oxiranyl}-methanol

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Technology Process of {(2R,3R)-3-[(S)-2-(4-Methoxy-benzyloxy)-1-methyl-ethyl]-2-methyl-oxiranyl}-methanol

There total 9 articles about {(2R,3R)-3-[(S)-2-(4-Methoxy-benzyloxy)-1-methyl-ethyl]-2-methyl-oxiranyl}-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 220213-54-7
(E)-(R)-5-(4-Methoxy-benzyloxy)-2,4-dimethyl-pent-2-en-1-ol

: 220213-63-8
{(2R,3R)-3-[(S)-2-(4-Methoxy-benzyloxy)-1-methyl-ethyl]-2-methyl-oxiranyl}-methanol

Guidance literature:: With titanium(IV) isopropylate; tert.-butylhydroperoxide; (-)-diethyl tartrate;
DOI:10.1016/S0040-4039(98)02110-8

Reference yield: 93.0%

: 220213-54-7
(E)-(R)-5-(4-Methoxy-benzyloxy)-2,4-dimethyl-pent-2-en-1-ol

: C₁₅H₂₂O₄

: 220213-63-8
{(2R,3R)-3-[(S)-2-(4-Methoxy-benzyloxy)-1-methyl-ethyl]-2-methyl-oxiranyl}-methanol

Guidance literature:: With titanium(IV) isopropylate; tert.-butylhydroperoxide; D-(-)-diisopropyl tartrate; In dichloromethane; at -78 - -25 ℃; optical yield given as %de; Molecular sieve;
DOI:10.1021/ja8063205

Reference yield:

: 132969-60-9
(2S)-3-[(4-methoxybenzyl)oxy]-2-methylpropanal

: 220213-63-8
{(2R,3R)-3-[(S)-2-(4-Methoxy-benzyloxy)-1-methyl-ethyl]-2-methyl-oxiranyl}-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / CH₂Cl₂ / 23 °C

2: Ti(O-i-Pr)4; TBHP; (-)-DIPT

With titanium(IV) isopropylate; tert.-butylhydroperoxide; D-(-)-diisopropyl tartrate; In dichloromethane; 1: Wittig reaction / 2: Sharpless asymmetric epoxidation;
DOI:10.1021/ol990572s